toluene-4-sulfonic acid 2-[[3-(3-chloro-phenyl)-2-hydroxy-3-(2-methoxy-phenoxy)-propyl]-(toluene-4-sulfonyl)-amino]-ethyl ester

Base Information

Chemical Name:toluene-4-sulfonic acid 2-[[3-(3-chloro-phenyl)-2-hydroxy-3-(2-methoxy-phenoxy)-propyl]-(toluene-4-sulfonyl)-amino]-ethyl ester
CAS No.:863969-85-1
Molecular Formula:C₃₂H₃₄ClNO₈S₂
Molecular Weight:660.209
Hs Code.:

Synonyms:

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Chemical Property of toluene-4-sulfonic acid 2-[[3-(3-chloro-phenyl)-2-hydroxy-3-(2-methoxy-phenoxy)-propyl]-(toluene-4-sulfonyl)-amino]-ethyl ester

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Technology Process of toluene-4-sulfonic acid 2-[[3-(3-chloro-phenyl)-2-hydroxy-3-(2-methoxy-phenoxy)-propyl]-(toluene-4-sulfonyl)-amino]-ethyl ester

There total 9 articles about toluene-4-sulfonic acid 2-[[3-(3-chloro-phenyl)-2-hydroxy-3-(2-methoxy-phenoxy)-propyl]-(toluene-4-sulfonyl)-amino]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 125617-30-3
rac-(3-(3-chlorophenyl)oxiran-2-yl)methanol

: 863969-85-1
toluene-4-sulfonic acid 2-[[3-(3-chloro-phenyl)-2-hydroxy-3-(2-methoxy-phenoxy)-propyl]-(toluene-4-sulfonyl)-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1.1: aq. NaOH; methyltributylammonium chloride / CH₂Cl₂ / 2 h / 20 °C

1.2: 39 percent / 3 h / 65 °C

2.1: Et₃N / ethyl acetate / 0.25 h / -20 °C

3.1: Et₃N / ethyl acetate / 0.25 h / -20 °C

4.1: aq. HCl / ethyl acetate / -20 - 20 °C

5.1: aq. NaOH; methyltributylammonium chloride / toluene / 20 °C

6.1: 48 percent / propan-2-ol / Heating

7.1: Et₃N / CH₂Cl₂

With hydrogenchloride; sodium hydroxide; triethylamine; methyl tributylammonium chloride; In dichloromethane; ethyl acetate; isopropyl alcohol; toluene;
DOI:10.1016/j.tetasy.2005.06.012

Reference yield:

: 863969-83-9
1,2-epoxy-3-[(3-chlorophenyl)-(2-methoxyphenoxy)]propane

: 863969-85-1
toluene-4-sulfonic acid 2-[[3-(3-chloro-phenyl)-2-hydroxy-3-(2-methoxy-phenoxy)-propyl]-(toluene-4-sulfonyl)-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / propan-2-ol / Heating

2: Et₃N / CH₂Cl₂

With triethylamine; In dichloromethane; isopropyl alcohol;
DOI:10.1016/j.tetasy.2005.06.012

Reference yield:

: 863969-82-8
3-(3-chlorophenyl)-3-(2-methoxyphenoxy)-propane-1,2-diol

: 863969-85-1
toluene-4-sulfonic acid 2-[[3-(3-chloro-phenyl)-2-hydroxy-3-(2-methoxy-phenoxy)-propyl]-(toluene-4-sulfonyl)-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: Et₃N / ethyl acetate / 0.25 h / -20 °C

2: Et₃N / ethyl acetate / 0.25 h / -20 °C

3: aq. HCl / ethyl acetate / -20 - 20 °C

4: aq. NaOH; methyltributylammonium chloride / toluene / 20 °C

5: 48 percent / propan-2-ol / Heating

6: Et₃N / CH₂Cl₂

With hydrogenchloride; sodium hydroxide; triethylamine; methyl tributylammonium chloride; In dichloromethane; ethyl acetate; isopropyl alcohol; toluene;
DOI:10.1016/j.tetasy.2005.06.012