Technology Process of C19H29N2O2P
There total 6 articles about C19H29N2O2P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
benzene-d6;
at 20 ℃;
for 2h;
Solvent;
Inert atmosphere;
Sealed tube;
DOI:10.1021/ja412469e
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene / 48 h / 80 °C / Inert atmosphere
2: hydrogen; palladium 10% on activated carbon / methanol / 18 h / 760.05 Torr / Inert atmosphere
3: potassium phosphate / water; dichloromethane / 2 h / Cooling with ice; Inert atmosphere
4: triethylamine; phosphorus trichloride / pentane / 6 h / -78 - 20 °C / Inert atmosphere
5: benzene-d6 / 2 h / 20 °C / Inert atmosphere; Sealed tube
With
potassium phosphate; palladium 10% on activated carbon; hydrogen; triethylamine; phosphorus trichloride;
In
methanol; dichloromethane; benzene-d6; water; toluene; pentane;
DOI:10.1021/ja412469e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium phosphate / water; dichloromethane / 2 h / Cooling with ice; Inert atmosphere
2: triethylamine; phosphorus trichloride / pentane / 6 h / -78 - 20 °C / Inert atmosphere
3: benzene-d6 / 2 h / 20 °C / Inert atmosphere; Sealed tube
With
potassium phosphate; triethylamine; phosphorus trichloride;
In
dichloromethane; benzene-d6; water; pentane;
DOI:10.1021/ja412469e
