Technology Process of C2HF3O2*C39H52N4O10S2
There total 13 articles about C2HF3O2*C39H52N4O10S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
BrH*C10H25N3O3S; C33H32N2O10S;
With
sodium hydrogencarbonate;
In
water; N,N-dimethyl-formamide;
at 20 ℃;
for 0.5h;
trifluoroacetic acid;
In
water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob00022a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2,6-di-tert-butyl-pyridine / 16 h / 155 °C / Inert atmosphere; Ionic liquid
2: hydrogenchloride / water / 3 h / Reflux; Inert atmosphere
3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 20 °C
4: sodium hydrogencarbonate / water; N,N-dimethyl-formamide / 0.5 h / 20 °C
With
hydrogenchloride; 2,6-di-tert-butyl-pyridine; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine;
In
water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob00022a
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: pyridine; p-toluenesulfonyl chloride / 4 h / 20 °C / Inert atmosphere
2.1: boron tribromide / dichloromethane / 4 h / 20 °C
2.2: 16 h / 0 - 20 °C
3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
4.1: 2,6-di-tert-butyl-pyridine / 16 h / 155 °C / Inert atmosphere; Ionic liquid
5.1: hydrogenchloride / water / 3 h / Reflux; Inert atmosphere
6.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 20 °C
7.1: sodium hydrogencarbonate / water; N,N-dimethyl-formamide / 0.5 h / 20 °C
With
pyridine; hydrogenchloride; 2,6-di-tert-butyl-pyridine; di-isopropyl azodicarboxylate; boron tribromide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
3.1: Mitsunobu reaction;
DOI:10.1039/c2ob00022a