[2,4,6-tri-tert-butylphenyl-P=C(Cl)]2SbCl

Base Information

Chemical Name:[2,4,6-tri-tert-butylphenyl-P=C(Cl)]2SbCl
CAS No.:1042440-30-1
Molecular Formula:C₃₈H₅₈Cl₃P₂Sb
Molecular Weight:804.935
Hs Code.:

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Chemical Property of [2,4,6-tri-tert-butylphenyl-P=C(Cl)]2SbCl

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Technology Process of [2,4,6-tri-tert-butylphenyl-P=C(Cl)]2SbCl

There total 1 articles about [2,4,6-tri-tert-butylphenyl-P=C(Cl)]2SbCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 10025-91-9
antimony(III) chloride

: 100281-24-1
2,2-dichloro-1-(2,4,6-tri-tert-butylphenyl)-1-phosphaethene

: 1042440-39-0
2,4,6-tri-tert-butylphenyl-P=C(Cl)SbCl₂

: 1042440-30-1
[2,4,6-tri-tert-butylphenyl-P=C(Cl)]2SbCl

: 1042440-29-8
[2,4,6-tri-tert-butylphenyl-P=C(Cl)]3Sb

Guidance literature:: With n-BuLi; In tetrahydrofuran; under N2 atm. to soln. Mes*P=CCl2 in THF at -78°C n-BuLi was added dropwise and stirred for 30 min, react. mixt. was added at -78°C to soln. SbCl3 in THF, stirred for 20 min and warmed to room temp.; solvent was removed in vacuo, crystn. from pentane;
DOI:10.1016/j.jorganchem.2008.04.012