Technology Process of C18H20FNO4
There total 3 articles about C18H20FNO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
mescaline hydrochloride;
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 0.5h;
4-fluorobenzoyl chloride;
In
dichloromethane;
at 20 ℃;
for 4h;
DOI:10.1002/ardp.201100169
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / Cooling with ice; Reflux
2.1: triethylamine / dichloromethane / 0.5 h / 20 °C
2.2: 4 h / 20 °C
With
lithium aluminium tetrahydride; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/ardp.201100169
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonium acetate; acetic acid / 3 h / Reflux
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / Cooling with ice; Reflux
3.1: triethylamine / dichloromethane / 0.5 h / 20 °C
3.2: 4 h / 20 °C
With
lithium aluminium tetrahydride; ammonium acetate; acetic acid; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/ardp.201100169