2-((tert-butoxycarbonyl)amino)ethyl ((2S,3R)-3-hydroxy-4-(N-((S)-2-methylbutyl)benzo[d]thiazole-6-sulfonamido)-1-phenylbutan-2-yl)carbamate

Base Information

Chemical Name:2-((tert-butoxycarbonyl)amino)ethyl ((2S,3R)-3-hydroxy-4-(N-((S)-2-methylbutyl)benzo[d]thiazole-6-sulfonamido)-1-phenylbutan-2-yl)carbamate
CAS No.:1386394-62-2
Molecular Formula:C₃₀H₄₂N₄O₇S₂
Molecular Weight:634.818
Hs Code.:

2-((tert-butoxycarbonyl)amino)ethyl ((2S,3R)-3-hydroxy-4-(N-((S)-2-methylbutyl)benzo[d]thiazole-6-sulfonamido)-1-phenylbutan-2-yl)carbamate

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Chemical Property of 2-((tert-butoxycarbonyl)amino)ethyl ((2S,3R)-3-hydroxy-4-(N-((S)-2-methylbutyl)benzo[d]thiazole-6-sulfonamido)-1-phenylbutan-2-yl)carbamate

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Technology Process of 2-((tert-butoxycarbonyl)amino)ethyl ((2S,3R)-3-hydroxy-4-(N-((S)-2-methylbutyl)benzo[d]thiazole-6-sulfonamido)-1-phenylbutan-2-yl)carbamate

There total 3 articles about 2-((tert-butoxycarbonyl)amino)ethyl ((2S,3R)-3-hydroxy-4-(N-((S)-2-methylbutyl)benzo[d]thiazole-6-sulfonamido)-1-phenylbutan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026701-90-5
C₂₂H₂₉N₃O₃S₂

: 92883-67-5
tert-butyl (2-((((2,5-dioxopyrrolidin-1-yl)oxy)carbonyl)oxy)ethyl)carbamate

: 1386394-62-2
2-((tert-butoxycarbonyl)amino)ethyl ((2S,3R)-3-hydroxy-4-(N-((S)-2-methylbutyl)benzo[d]thiazole-6-sulfonamido)-1-phenylbutan-2-yl)carbamate

Guidance literature:: C₂₂H₂₉N₃O₃S₂; With tertiary amine; In tetrahydrofuran; at 0 ℃; for 0.166667h;

tert-butyl (2-((((2,5-dioxopyrrolidin-1-yl)oxy)carbonyl)oxy)ethyl)carbamate; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jm300238h

Reference yield:

: 1026701-54-1
tert-butyl ((2S,3R)-3-hydroxy-4-(N-((2S)-2-methylbutyl)benzo[d]thiazole-6-sulfonamido)-1-phenylbutan-2-yl)carbamate

: 1386394-62-2
2-((tert-butoxycarbonyl)amino)ethyl ((2S,3R)-3-hydroxy-4-(N-((S)-2-methylbutyl)benzo[d]thiazole-6-sulfonamido)-1-phenylbutan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 20 °C

2.1: tertiary amine / tetrahydrofuran / 0.17 h / 0 °C

2.2: 0 - 20 °C

With trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm300238h

Reference yield:

: 26690-80-2
2-(N-tert-butoxycarbonylamino)ethanol

: 1386394-62-2
2-((tert-butoxycarbonyl)amino)ethyl ((2S,3R)-3-hydroxy-4-(N-((S)-2-methylbutyl)benzo[d]thiazole-6-sulfonamido)-1-phenylbutan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / acetonitrile / 8 h

2.1: tertiary amine / tetrahydrofuran / 0.17 h / 0 °C

2.2: 0 - 20 °C

With triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm300238h