(2S,4S)-1-benzyl-2.4-dimethylazetidine

Base Information

Chemical Name:(2S,4S)-1-benzyl-2.4-dimethylazetidine
CAS No.:55423-35-3
Molecular Formula:C₁₂H₁₇N
Molecular Weight:175.274
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S)-1-benzyl-2.4-dimethylazetidine

Chemical Property:

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Technology Process of (2S,4S)-1-benzyl-2.4-dimethylazetidine

There total 6 articles about (2S,4S)-1-benzyl-2.4-dimethylazetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 56198-29-9
(2R,4R)-pentane-2,4-diyl bis(methanesulfonate)

: 100-46-9
benzylamine

: 55423-35-3,55423-36-4
(2S,4S)-1-benzyl-2.4-dimethylazetidine

Guidance literature:: at 45 ℃; for 60h;
DOI:10.1002/(sici)1099-0690(200005)2000:9<1815::aid-ejoc1815>3.0.co;2-8

Reference yield:

: 42075-32-1
(2R,4R)-pentanediol

: 55423-35-3,55423-36-4
(2S,4S)-1-benzyl-2.4-dimethylazetidine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1 h / 0 °C

2: 60 percent / 60 h / 45 °C

With triethylamine; In dichloromethane; 1: Acylation / 2: Cyclization;
DOI:10.1002/(sici)1099-0690(200005)2000:9<1815::aid-ejoc1815>3.0.co;2-8

Reference yield:

: C₁₆H₂₆NO₄P

: 55423-35-3,55423-36-4
(2S,4S)-1-benzyl-2.4-dimethylazetidine

: 286435-24-3
C₁₂H₁₇N

: C₁₂H₁₇N

Guidance literature:: With R-B-isopinocampheyl-9-borabicyclo[3.3.1]nonane; In tetrahydrofuran; at 60 ℃; optical yield given as %ee; stereoselective reaction;
DOI:10.1055/s-0031-1290954