Technology Process of 9,10-bis(4-(6-hydroxyhexyl)oxyphenyl)anthracene
There total 3 articles about 9,10-bis(4-(6-hydroxyhexyl)oxyphenyl)anthracene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; potassium iodide;
In
acetonitrile;
for 96h;
Reflux;
DOI:10.1007/s11164-012-0658-y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; water / 48 h / 80 °C / Inert atmosphere
2: boron tribromide; water / dichloromethane; hexane / 0 °C / Inert atmosphere
3: potassium carbonate; potassium iodide / acetonitrile / 96 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); water; boron tribromide; sodium carbonate; potassium carbonate; potassium iodide;
In
hexane; dichloromethane; water; toluene; acetonitrile;
DOI:10.1007/s11164-012-0658-y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; water / 48 h / 80 °C / Inert atmosphere
2: boron tribromide; water / dichloromethane; hexane / 0 °C / Inert atmosphere
3: potassium carbonate; potassium iodide / acetonitrile / 96 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); water; boron tribromide; sodium carbonate; potassium carbonate; potassium iodide;
In
hexane; dichloromethane; water; toluene; acetonitrile;
DOI:10.1007/s11164-012-0658-y