benzyl 3-{(4-{[[(7-azidoheptanoyl)amino](benzyloxy)acetyl]amino}butyl)[(benzyloxy)carbonyl]amino}propyl carbamate

Base Information

Chemical Name:benzyl 3-{(4-{[[(7-azidoheptanoyl)amino](benzyloxy)acetyl]amino}butyl)[(benzyloxy)carbonyl]amino}propyl carbamate
CAS No.:343626-01-7
Molecular Formula:C₃₉H₅₁N₇O₇
Molecular Weight:729.877
Hs Code.:

Synonyms:

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Chemical Property of benzyl 3-{(4-{[[(7-azidoheptanoyl)amino](benzyloxy)acetyl]amino}butyl)[(benzyloxy)carbonyl]amino}propyl carbamate

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Technology Process of benzyl 3-{(4-{[[(7-azidoheptanoyl)amino](benzyloxy)acetyl]amino}butyl)[(benzyloxy)carbonyl]amino}propyl carbamate

There total 5 articles about benzyl 3-{(4-{[[(7-azidoheptanoyl)amino](benzyloxy)acetyl]amino}butyl)[(benzyloxy)carbonyl]amino}propyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97628-87-0
benzyl (4-aminobutyl)(3-(((benzyloxy)carbonyl)amino)propyl)carbamate

: 181484-31-1
(7-azido-heptanoylamino)-benzyloxy-acetic acid

: 343626-01-7
benzyl 3-{(4-{[[(7-azidoheptanoyl)amino](benzyloxy)acetyl]amino}butyl)[(benzyloxy)carbonyl]amino}propyl carbamate

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1016/S0040-4020(01)00130-2

Reference yield:

: 181483-85-2
7-azidoheptanamide

: 343626-01-7
benzyl 3-{(4-{[[(7-azidoheptanoyl)amino](benzyloxy)acetyl]amino}butyl)[(benzyloxy)carbonyl]amino}propyl carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: molecular sieves / CH₂Cl₂ / 24 h / Heating

2: SOCl₂ / CH₂Cl₂ / 2 h / Heating

3: 13.4 g / Et₃N / CH₂Cl₂ / 24 h / 20 °C

4: 1N NaOH / 1,2-dimethoxy-ethane / 1.5 h / 20 °C

5: 17.5 g / DCC; HOBT / CH₂Cl₂ / 20 h / 20 °C

With sodium hydroxide; thionyl chloride; molecular sieve; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1016/S0040-4020(01)00130-2

Reference yield:

: (7-azido-heptanoylamino)-chloro-acetic acid methyl ester

: 343626-01-7
benzyl 3-{(4-{[[(7-azidoheptanoyl)amino](benzyloxy)acetyl]amino}butyl)[(benzyloxy)carbonyl]amino}propyl carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 13.4 g / Et₃N / CH₂Cl₂ / 24 h / 20 °C

2: 1N NaOH / 1,2-dimethoxy-ethane / 1.5 h / 20 °C

3: 17.5 g / DCC; HOBT / CH₂Cl₂ / 20 h / 20 °C

With sodium hydroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1016/S0040-4020(01)00130-2