Technology Process of 4,6-dimethoxy-3,5-di<3-2H>methyl-2-(1-methyl-2-oxopropyl)benzaldehyde
There total 9 articles about 4,6-dimethoxy-3,5-di<3-2H>methyl-2-(1-methyl-2-oxopropyl)benzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dimethylsulfide; ozone;
In
ethyl acetate;
at -78 ℃;
for 0.166667h;
DOI:10.1039/P19810001685
- Guidance literature:
-
Multi-step reaction with 6 steps
1: lithium aluminium deuteride / diethyl ether / 3 h / Ambient temperature
2: hydrogen / palladium oxide / acetic acid
3: stannic chloride / CS2 / 2 h / Heating
4: lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature
5: toluene-p-sulphonic acid / 130 - 140 °C / 0.4 Torr
6: ozone, dimethyl sulphide / ethyl acetate / 0.17 h / -78 °C
With
lithium aluminium tetrahydride; lithium aluminium deuteride; dimethylsulfide; hydrogen; tin(IV) chloride; toluene-4-sulfonic acid; ozone;
palladium(II) oxide;
In
carbon disulfide; diethyl ether; acetic acid; ethyl acetate;
DOI:10.1039/P19810001685
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 1.) hydrogen chloride gas, 2.) water / 1.) ether, 45 min, 2.) 40 deg C
2: 92 percent / potassium carbonate / acetone / 5 h / Heating
3: lithium aluminium deuteride / diethyl ether / 3 h / Ambient temperature
4: hydrogen / palladium oxide / acetic acid
5: stannic chloride / CS2 / 2 h / Heating
6: lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature
7: toluene-p-sulphonic acid / 130 - 140 °C / 0.4 Torr
8: ozone, dimethyl sulphide / ethyl acetate / 0.17 h / -78 °C
With
hydrogenchloride; lithium aluminium tetrahydride; lithium aluminium deuteride; dimethylsulfide; water; hydrogen; tin(IV) chloride; potassium carbonate; toluene-4-sulfonic acid; ozone;
palladium(II) oxide;
In
carbon disulfide; diethyl ether; acetic acid; ethyl acetate; acetone;
DOI:10.1039/P19810001685
