(2-Acetoxymethyl-1,3-diacetoxy-2-propyl)amide of 4-phenylacetic acid

Base Information

Chemical Name:(2-Acetoxymethyl-1,3-diacetoxy-2-propyl)amide of 4-phenylacetic acid
CAS No.:79567-53-6
Molecular Formula:C₂₂H₃₀Cl₂N₂O₇
Molecular Weight:505.395
Hs Code.:

(2-Acetoxymethyl-1,3-diacetoxy-2-propyl)amide of 4-<di(2-chloroethyl)amino>phenylacetic acid

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Chemical Property of (2-Acetoxymethyl-1,3-diacetoxy-2-propyl)amide of 4-phenylacetic acid

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Technology Process of (2-Acetoxymethyl-1,3-diacetoxy-2-propyl)amide of 4-phenylacetic acid

There total 3 articles about (2-Acetoxymethyl-1,3-diacetoxy-2-propyl)amide of 4-phenylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 64205-65-8
(2-Hydroxymethyl-1,3-dihydroxy-2-propyl)amide of 4-phenylacetic acid

: 75-36-5
acetyl chloride

: 79567-53-6
(2-Acetoxymethyl-1,3-diacetoxy-2-propyl)amide of 4-phenylacetic acid

Guidance literature:: for 2h; Heating;
DOI:10.1007/BF00758456

Reference yield:

: 10477-72-2
4-bis(2-chloroethyl)aminophenylacetic acid

: 79567-53-6
(2-Acetoxymethyl-1,3-diacetoxy-2-propyl)amide of 4-phenylacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂

2: 50 percent / H₂O; acetone / 0.25 h / -10 °C

3: 78 percent / 2 h / Heating

With thionyl chloride; In water; acetone;
DOI:10.1007/BF00758456

Reference yield:

: 53039-95-5
p-phenylacetyl chloride hydrochloride

: 79567-53-6
(2-Acetoxymethyl-1,3-diacetoxy-2-propyl)amide of 4-phenylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / H₂O; acetone / 0.25 h / -10 °C

2: 78 percent / 2 h / Heating

In water; acetone;
DOI:10.1007/BF00758456