Technology Process of 1-(2-formyl-6-iodophenyl)-2-naphthaldehyde
There total 6 articles about 1-(2-formyl-6-iodophenyl)-2-naphthaldehyde which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
silver nitrate;
In
1,4-dioxane;
at 100 ℃;
for 15h;
DOI:10.1039/b208871a
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 43 percent / Cu bronze / 20 h / 200 °C
2.1: 87 percent / SnCl2*2H2O / ethyl acetate / 15 h / 80 °C
3.1: H2SO4; NaNO2 / 0.25 h / -10 °C
3.2: 57 percent / aq. KI / 15 h / -10 - 20 °C
4.1: NBS; benzoyl peroxide / CCl4 / 48 h / 80 °C / Heating; irradiation
5.1: 0.154 g / aq. AgNO3 / dioxane / 15 h / 100 °C
With
N-Bromosuccinimide; copper bronze; sulfuric acid; silver nitrate; tin(ll) chloride; sodium nitrite; dibenzoyl peroxide;
In
1,4-dioxane; tetrachloromethane; ethyl acetate;
1.1: Ullmann reaction / 3.2: Sandmeyer reaction;
DOI:10.1039/b208871a
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 43 percent / Cu bronze / 20 h / 200 °C
2.1: 87 percent / SnCl2*2H2O / ethyl acetate / 15 h / 80 °C
3.1: H2SO4; NaNO2 / 0.25 h / -10 °C
3.2: 57 percent / aq. KI / 15 h / -10 - 20 °C
4.1: NBS; benzoyl peroxide / CCl4 / 48 h / 80 °C / Heating; irradiation
5.1: 0.154 g / aq. AgNO3 / dioxane / 15 h / 100 °C
With
N-Bromosuccinimide; copper bronze; sulfuric acid; silver nitrate; tin(ll) chloride; sodium nitrite; dibenzoyl peroxide;
In
1,4-dioxane; tetrachloromethane; ethyl acetate;
1.1: Ullmann reaction / 3.2: Sandmeyer reaction;
DOI:10.1039/b208871a
