C₃₆H₃₇F₃N₂O₅

Base Information

Chemical Name:C₃₆H₃₇F₃N₂O₅
CAS No.:1416772-57-0
Molecular Formula:C₃₆H₃₇F₃N₂O₅
Molecular Weight:634.695
Hs Code.:

C<sub>36</sub>H<sub>37</sub>F<sub>3</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₃₆H₃₇F₃N₂O₅

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Technology Process of C₃₆H₃₇F₃N₂O₅

There total 15 articles about C₃₆H₃₇F₃N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 20445-31-2
R-(+)-α-trifluoromethyl-α-methoxy-phenylacetic acid

: 1416772-56-9
C₂₆H₃₀N₂O₃

: 1416772-57-0
C₃₆H₃₇F₃N₂O₅

Guidance literature:: With dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In toluene; at 20 - 45 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ml300385q

Reference yield:

: 115167-43-6
methyl (Z)-2-acetamido-3-(3-pyridyl)propenoate

: 1416772-57-0
C₃₆H₃₇F₃N₂O₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

2.1: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

3.1: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

4.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

5.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

6.1: chromium dichloride / tetrahydrofuran / 0.42 h / 200 °C / Inert atmosphere; Schlenk technique

6.2: 3 h / 20 °C

7.1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 72 h / 20 °C / Inert atmosphere; Schlenk technique

8.1: sodium periodate / dichloromethane; water / 2 h / 20 °C / Inert atmosphere; Schlenk technique

9.1: 2,3-Dimethyl-2-butene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 0.75 h / 20 °C / Inert atmosphere; Schlenk technique

10.1: methanol; diethyl ether; toluene / 0.08 h / 0 °C / Inert atmosphere; Schlenk technique

11.1: triethylamine; dmap; 2,4,6-trichlorobenzoyl chloride / toluene / 24 h / 20 - 45 °C / Inert atmosphere; Schlenk technique

With chromium dichloride; dmap; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; lithium aluminium tetrahydride; tetrafluoroboric acid; thionyl chloride; 2,3-Dimethyl-2-butene; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; methanesulfonamide; 2,4,6-trichlorobenzoyl chloride; AD-mix-α; hydrogen; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1021/ml300385q

Reference yield:

: 89890-92-6
N-acetyl-(β-3-pyridyl)-α,β-dehydroalanine

: 1416772-57-0
C₃₆H₃₇F₃N₂O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium acetate / 72 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

3.1: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

4.1: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

5.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

6.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

7.1: triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane / dichloromethane; hexane / 3 h / -78 °C / Inert atmosphere; Schlenk technique

7.2: 4.3 h / -78 - 0 °C

8.1: lithium hydroxide monohydrate / methanol; tetrahydrofuran; water / 24 h / 20 °C / Inert atmosphere; Schlenk technique

9.1: methanol; diethyl ether; toluene / 0.08 h / 0 °C / Inert atmosphere; Schlenk technique

10.1: triethylamine; dmap; 2,4,6-trichlorobenzoyl chloride / toluene / 24 h / 20 - 45 °C / Inert atmosphere; Schlenk technique

With dmap; lithium aluminium tetrahydride; tetrafluoroboric acid; thionyl chloride; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; hydrogen; sodium acetate; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; toluene;
DOI:10.1021/ml300385q