cis-[Pd(2,3,5,6-tetrafluorobenzenethiolate)2(1,2-bis(diphenylphosphino)ethane)]

Base Information

Chemical Name:cis-[Pd(2,3,5,6-tetrafluorobenzenethiolate)2(1,2-bis(diphenylphosphino)ethane)]
CAS No.:515843-00-2
Molecular Formula:C₃₈H₂₆F₈P₂PdS₂
Molecular Weight:867.111
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-[Pd(2,3,5,6-tetrafluorobenzenethiolate)2(1,2-bis(diphenylphosphino)ethane)]

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Technology Process of cis-[Pd(2,3,5,6-tetrafluorobenzenethiolate)2(1,2-bis(diphenylphosphino)ethane)]

There total 1 articles about cis-[Pd(2,3,5,6-tetrafluorobenzenethiolate)2(1,2-bis(diphenylphosphino)ethane)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 19978-61-1
(1,2-bis(diphenylphosphanyl)ethane)dichloridopalladium(II)

: 107700-90-3
thallium p-tetrafluorobenzenethiolate

: 515843-00-2
cis-[Pd(2,3,5,6-tetrafluorobenzenethiolate)2(1,2-bis(diphenylphosphino)ethane)]

Guidance literature:: In acetone; byproducts: TlCl; to suspn. of dichloro(diphosphino)metal(II) complex in acetone added Tl(SC6F4H); stirred for 18 h at room temp.; TlCl filtered off; solvent evapd. (vac.); hexane added; solid filtered off; washed (hexane); dried (vac.); elem. anal.;
DOI:10.1016/S0022-328X(02)01734-5

Reference yield: 71.0%

: cis-[(pentafluorophenyl)2 (tetrahydrofurane)2 platinum(II)]

: 515843-00-2
cis-[Pd(2,3,5,6-tetrafluorobenzenethiolate)2(1,2-bis(diphenylphosphino)ethane)]

: 515843-08-0,515843-06-8
[(pentafluorophenyl)2Pt(μ-2,3,5,6-tetrafluorobenzenethiolate)2Pd(1,2-bis(diphenylphosphino)ethane)]

Guidance literature:: In dichloromethane; byproducts: THF; Pt(C6F5)2(THF)2 added to soln. of bis(tetrafluorothiophenolato)phosphino-metal(II) complex in CH2Cl2; stirred for 6 h at room temp.; soln. evapd. to dryness; MeOH added; solid filtered off; washed (MeOH); dried (vac., P2O5); elem. anal.;
DOI:10.1016/S0022-328X(02)01734-5

Reference yield: 60.0%

: cis-[Pd(pentafluorophenyl)2(THF)2]

: 515843-00-2
cis-[Pd(2,3,5,6-tetrafluorobenzenethiolate)2(1,2-bis(diphenylphosphino)ethane)]

: 515843-05-7
[(pentafluorophenyl)2Pd(μ-2,3,5,6-tetrafluorobenzenethiolate)2Pd(1,2-bis(diphenylphosphino)ethane)]

Guidance literature:: In dichloromethane; byproducts: THF; Pd(C6F5)2(THF)2 added to soln. of bis(tetrafluorothiophenolato)phosphino-metal(II) complex in CH2Cl2; stirred for 6 h at room temp.; soln. evapd. to dryness; MeOH added; solid filtered off; washed (MeOH); dried (vac., P2O5); elem. anal.;
DOI:10.1016/S0022-328X(02)01734-5