bis(tris(trimethylsilyl)methyl)bis(μ-benzoate-O,O')diindium(II) diiodide diisopropyl ester

Base Information

• Chemical Name: bis(tris(trimethylsilyl)methyl)bis(μ-benzoate-O,O')diindium(II) diiodide diisopropyl ester
• CAS No.: 736155-19-4
• Molecular Formula: C₆H₁₄O*C₃₄H₆₄In₂O₄Si₆
• Molecular Weight: 1037.21
• Mol file: 736155-19-4.mol

Synonyms:

Chemical Property of bis(tris(trimethylsilyl)methyl)bis(μ-benzoate-O,O')diindium(II) diiodide diisopropyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(tris(trimethylsilyl)methyl)bis(μ-benzoate-O,O')diindium(II) diiodide diisopropyl ester

There total 1 articles about bis(tris(trimethylsilyl)methyl)bis(μ-benzoate-O,O')diindium(II) diiodide diisopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

tris(tris(trimethylsilyl)methyl)diindium diiodide + di-isopropyl ether (108-20-3) + silver benzoate (532-31-0) → bis(tris(trimethylsilyl)methyl)bis(μ-benzoate-O,O')diindium(II) diiodide diisopropyl ester (736155-19-4)

Guidance literature:

In toluene; byproducts: AgI; Ar, a soln. of Ga compd. added to a soln. of Ag compd. at -90°C, stirred, slowly warmed to -65°C; ppt. filtered (-70°C), solvent removed (vac., room temp.), recrystd. (diisopropyl ester);

DOI:10.1002/ejic.200300640

upstream raw materials:

di-isopropyl ether

silver benzoate