C₃₀H₄₂N₅O⁽¹⁺⁾*Cl^(1-)

Base Information

Chemical Name:C₃₀H₄₂N₅O⁽¹⁺⁾*Cl^(1-)
CAS No.:1604799-68-9
Molecular Formula:C₃₀H₄₂N₅O*Cl
Molecular Weight:524.149
Hs Code.:

C<sub>30</sub>H<sub>42</sub>N<sub>5</sub>O<sup>(1+)</sup>*Cl<sup>(1-)</sup>

Synonyms:

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Chemical Property of C₃₀H₄₂N₅O⁽¹⁺⁾*Cl^(1-)

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Technology Process of C₃₀H₄₂N₅O⁽¹⁺⁾*Cl^(1-)

There total 9 articles about C₃₀H₄₂N₅O⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(4-Azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl)ethane-1,2-diamine dihydrochloride

: (N-(2,6-Diisopropylphenyl)-N′-[4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)-2,6-diisopropylphenyl]imidazolin-2-ylidene)-chlorogold(I)

: 1604799-68-9
C₃₀H₄₂N₅O⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1: orthoformic acid triethyl ester; formic acid / ethanol / 2 h / Reflux

2: ammonium hydroxide / water / 2 h / 20 °C / Inert atmosphere

3: acetonitrile / 16 h / 50 °C

4: dichloromethane / 16 h / 50 °C

With ammonium hydroxide; formic acid; orthoformic acid triethyl ester; In ethanol; dichloromethane; water; acetonitrile;
DOI:10.1039/c4dt00429a

Reference yield:

: 1604799-63-4
N-(4-azido-2,6-diisopropylphenyl)-N′-(2,6-diisopropylphenyl) imidazolinium chloride

: (N-(2,6-Diisopropylphenyl)-N′-[4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)-2,6-diisopropylphenyl]imidazolin-2-ylidene)-chlorogold(I)

: 1604799-68-9
C₃₀H₄₂N₅O⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium hydroxide / water / 2 h / 20 °C / Inert atmosphere

2: acetonitrile / 16 h / 50 °C

3: dichloromethane / 16 h / 50 °C

With ammonium hydroxide; In dichloromethane; water; acetonitrile;
DOI:10.1039/c4dt00429a

Reference yield:

: 2-((2,6-diisopropylphenyl)amino)-2-oxoacetyl chloride

: (N-(2,6-Diisopropylphenyl)-N′-[4-(4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl)-2,6-diisopropylphenyl]imidazolin-2-ylidene)-chlorogold(I)

: 1604799-68-9
C₃₀H₄₂N₅O⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium carbonate / dichloromethane / 2 h / 20 °C

2.1: sodium tetrahydroborate; trifluoroborane diethyl ether / tetrahydrofuran / 2 h / 29 °C

3.1: sodium hydrogencarbonate / water

3.2: 3 h / 70 °C / Inert atmosphere

4.1: orthoformic acid triethyl ester; formic acid / ethanol / 2 h / Reflux

5.1: ammonium hydroxide / water / 2 h / 20 °C / Inert atmosphere

6.1: acetonitrile / 16 h / 50 °C

7.1: dichloromethane / 16 h / 50 °C

With ammonium hydroxide; sodium tetrahydroborate; formic acid; trifluoroborane diethyl ether; sodium hydrogencarbonate; sodium carbonate; orthoformic acid triethyl ester; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1039/c4dt00429a