1-(cyclohexyl)-3-ferrocenylethylimidazolium iodide

Base Information

• Chemical Name: 1-(cyclohexyl)-3-ferrocenylethylimidazolium iodide
• CAS No.: 922192-61-8
• Molecular Formula: C₂₁H₂₇FeN₂*I
• Molecular Weight: 490.21
• Mol file: 922192-61-8.mol

Synonyms:

Chemical Property of 1-(cyclohexyl)-3-ferrocenylethylimidazolium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(cyclohexyl)-3-ferrocenylethylimidazolium iodide

There total 1 articles about 1-(cyclohexyl)-3-ferrocenylethylimidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1-ferrocenylethyl acetate + sodium iodide (7681-82-5,24359-64-6,41927-88-2,115813-40-6) + N-cyclohexylimidazole (67768-61-0) → 1-(cyclohexyl)-3-ferrocenylethylimidazolium iodide (922192-61-8)

Guidance literature:

In ethanol; water; acetonitrile; under N2, Schlenk techniques; Fe compd. and ligand (1:1.2 molar ratio) stirred for 24 h at 23°C, evapd., ethanolic soln. of NaI (5 equiv.) added, stored for 24 h; evapd., dissolved (CH2Cl2), filtered (celite), chromd. (silica, CH2Cl2/MeOH=96:4);

DOI:10.1016/j.molcata.2006.01.034

upstream raw materials:

sodium iodide

N-cyclohexylimidazole

Refernces