(E)-7-iodo-1-(p-tolylsulfonyl)-1,2,3,4,5,8-hexahydro-1H-azocine

Base Information

Chemical Name:(E)-7-iodo-1-(p-tolylsulfonyl)-1,2,3,4,5,8-hexahydro-1H-azocine
CAS No.:132937-98-5
Molecular Formula:C₁₄H₁₈INO₂S
Molecular Weight:391.273
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-7-iodo-1-(p-tolylsulfonyl)-1,2,3,4,5,8-hexahydro-1H-azocine

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Technology Process of (E)-7-iodo-1-(p-tolylsulfonyl)-1,2,3,4,5,8-hexahydro-1H-azocine

There total 3 articles about (E)-7-iodo-1-(p-tolylsulfonyl)-1,2,3,4,5,8-hexahydro-1H-azocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 107970-42-3
N-(hepta-5,6-dien-1-yl)-4-methylbenzenesulfonamide

: 132937-98-5
(E)-7-iodo-1-(p-tolylsulfonyl)-1,2,3,4,5,8-hexahydro-1H-azocine

: 2-(1-iodovinyl)-1-(p-tolylsulfonyl)piperidine

: 132928-10-0
(Z,Z)-3,11-diiodo-N,N-bis(p-tolylsulfonyl)-1,9-diazacyclohexadeca-3,11-diene

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; iodine; sodium hydride; Product distribution; multistep reaction: 1.) THF, room temperature, 1 h, 2.) 25 h; allene-based cyclisation via allylic iodide, effect of ring size on the product distribution;

Reference yield:

: (E)/(Z)-6,7-diiodo-N-(p-tolylsulfonyl)hept-5-enylamine

: 132937-98-5
(E)-7-iodo-1-(p-tolylsulfonyl)-1,2,3,4,5,8-hexahydro-1H-azocine

: 2-(1-iodovinyl)-1-(p-tolylsulfonyl)piperidine

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium hydride; In tetrahydrofuran; Yield given. Yields of byproduct given;

Reference yield:

: (E)/(Z)-6,7-diiodo-N-(p-tolylsulfonyl)hept-5-enylamine

: 132937-98-5
(E)-7-iodo-1-(p-tolylsulfonyl)-1,2,3,4,5,8-hexahydro-1H-azocine

: 2-(1-iodovinyl)-1-(p-tolylsulfonyl)piperidine

: 132928-10-0
(Z,Z)-3,11-diiodo-N,N-bis(p-tolylsulfonyl)-1,9-diazacyclohexadeca-3,11-diene

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium hydride; In tetrahydrofuran; for 25h; Yield given. Yields of byproduct given;