RuCl₂((C₆H₅)2PCH₂CH₂OCH₃)2

Base Information

Chemical Name:RuCl₂((C₆H₅)2PCH₂CH₂OCH₃)2
CAS No.:109011-62-3
Molecular Formula:C₃₀H₃₄Cl₂O₂P₂Ru
Molecular Weight:660.522
Hs Code.:

RuCl<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>OCH<sub>3</sub>)2

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Chemical Property of RuCl₂((C₆H₅)2PCH₂CH₂OCH₃)2

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Technology Process of RuCl₂((C₆H₅)2PCH₂CH₂OCH₃)2

There total 1 articles about RuCl₂((C₆H₅)2PCH₂CH₂OCH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: tris(triphenylphosphine)ruthenium(II) chloride

: 68899-50-3
(2-methoxyethyl)diphenylphosphine

: 109011-62-3
trans-dichlorobis((2-methoxyethyl)diphenylphosphine-O,P)ruthenium(II)

Guidance literature:: In dichloromethane; (dry, oxygen-free argon; Schlenk-technique); the ligand is added to the ruthenium complex in CH2Cl2, the soln. is refluxed for 10 min; evapn. to a low volume (vac.), addn. of diethyl ether,, filtn., washing with ether, drying in vacuo;

Reference yield: 96.0%

: 109011-62-3
bis(η2-O,P-(CH3OCH2CH2P(C6H5)2))dichloro ruthenium(II)

: 109-76-2,54018-94-9
Trimethylenediamine

: 396130-64-6
[RuCl2(η1-Ph2PCH2CH2OCH3)2(1,3-diaminopropane)]

Guidance literature:: In dichloromethane; (Ar); using Schlenk tecnhiques; addn. dropwise of soln. of NH2(CH2)3NH2 in CH2Cl2 to stirred soln. of RuCl2(PPh2C2H4OMe)2 in CH2Cl2; stirring atroom temp. for 45 min; concn. under reduced pressure, addn. of n-hexane, pptn., filtration, washing with n-hexane, drying under vac., elem. anal.;
DOI:10.1021/om0105831

Reference yield: 96.0%

: 109011-62-3
trans-dichlorobis((2-methoxyethyl)diphenylphosphine-O,P)ruthenium(II)

: 694-83-7
rac-diaminocyclohexane

: 620945-35-9,620949-90-8
RuCl₂((C₆H₅)2PCH₂CH₂OCH₃)2(H₂NC₆H₁₀NH₂)

Guidance literature:: In dichloromethane; a soln. of the diamine ligand (10% excess) in CH2Cl2 was added dropwise under Ar to a stirred soln. of Ru-complex in CH2Cl2, the mixt. was stirred for approx. 45 min at room temp.; filtd., concd., Et2O was added, ppt. was filtd. off, dissolved in CH2Cl2, concd., n-hexane was added, ppt. was collected by filtn., washed with n-hexane and dried under vac.; elem. anal.;
DOI:10.1016/S0020-1693(02)01535-9