4-(4,4-diphenyl-butyl)-piperazine-1-carboxylic acid ethyl ester

Base Information

Chemical Name:4-(4,4-diphenyl-butyl)-piperazine-1-carboxylic acid ethyl ester
CAS No.:103870-65-1
Molecular Formula:C₂₃H₃₀N₂O₂
Molecular Weight:366.503
Hs Code.:

Synonyms:

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Chemical Property of 4-(4,4-diphenyl-butyl)-piperazine-1-carboxylic acid ethyl ester

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Technology Process of 4-(4,4-diphenyl-butyl)-piperazine-1-carboxylic acid ethyl ester

There total 10 articles about 4-(4,4-diphenyl-butyl)-piperazine-1-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86419-96-7
2-(2,2-diphenyl-ethyl)-malonic acid

: 103870-65-1
4-(4,4-diphenyl-butyl)-piperazine-1-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 180 °C

2: sulfuric acid / CHCl₃ / 5 h / Heating

3: lithium aluminum hydride / diethyl ether / 20 °C

4: triethylamine / CHCl₃ / 24 h / 20 °C

5: 8 h / 100 °C

With lithium aluminium tetrahydride; sulfuric acid; triethylamine; In diethyl ether; chloroform;
DOI:10.1016/j.bmc.2007.01.024

Reference yield:

: 117-34-0
2,2-diphenylacetic acid

: 103870-65-1
4-(4,4-diphenyl-butyl)-piperazine-1-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 10 steps

1.1: sulfuric acid / CHCl₃ / 5 h / Heating

2.1: lithium aluminum hydride / diethyl ether / 4 h / 20 °C

3.1: triethylamine / CHCl₃ / 24 h / 20 °C

4.1: sodium / ethanol

4.2: ethanol / 10 h / Heating

5.1: KOH / ethanol / 10 h / Heating

6.1: 180 °C

7.1: sulfuric acid / CHCl₃ / 5 h / Heating

8.1: lithium aluminum hydride / diethyl ether / 20 °C

9.1: triethylamine / CHCl₃ / 24 h / 20 °C

10.1: 8 h / 100 °C

With potassium hydroxide; lithium aluminium tetrahydride; sulfuric acid; sodium; triethylamine; In diethyl ether; ethanol; chloroform;
DOI:10.1016/j.bmc.2007.01.024

Reference yield:

: 1883-32-5
2,2-diphenyl ethanol

: 103870-65-1
4-(4,4-diphenyl-butyl)-piperazine-1-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / CHCl₃ / 24 h / 20 °C

2.1: sodium / ethanol

2.2: ethanol / 10 h / Heating

3.1: KOH / ethanol / 10 h / Heating

4.1: 180 °C

5.1: sulfuric acid / CHCl₃ / 5 h / Heating

6.1: lithium aluminum hydride / diethyl ether / 20 °C

7.1: triethylamine / CHCl₃ / 24 h / 20 °C

8.1: 8 h / 100 °C

With potassium hydroxide; lithium aluminium tetrahydride; sulfuric acid; sodium; triethylamine; In diethyl ether; ethanol; chloroform;
DOI:10.1016/j.bmc.2007.01.024