Technology Process of C48H57NO12
There total 5 articles about C48H57NO12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) O3, 2.) Zn / 1.) CH2Cl2, -70 deg C, 1 h, 2.) CH2Cl2, from -70 deg C to RT, 2 h
2: aq. KHCO3 / methanol / 14 h
3: lithium tri-tert-butoxyaluminum hydride / diethyl ether / 1 h
4: aq. NaIO4 / ethanol / 1 h
5: 460 mg / KF / propan-2-ol / 14 h
With
potassium fluoride; sodium periodate; lithium tri(t-butoxy)aluminum hydride; potassium hydrogencarbonate; ozone; zinc;
In
methanol; diethyl ether; ethanol; isopropyl alcohol;
DOI:10.1021/jm00053a006
- Guidance literature:
-
Multi-step reaction with 2 steps
1: aq. NaIO4 / ethanol / 1 h
2: 460 mg / KF / propan-2-ol / 14 h
With
potassium fluoride; sodium periodate;
In
ethanol; isopropyl alcohol;
DOI:10.1021/jm00053a006
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium tri-tert-butoxyaluminum hydride / diethyl ether / 1 h
2: aq. NaIO4 / ethanol / 1 h
3: 460 mg / KF / propan-2-ol / 14 h
With
potassium fluoride; sodium periodate; lithium tri(t-butoxy)aluminum hydride;
In
diethyl ether; ethanol; isopropyl alcohol;
DOI:10.1021/jm00053a006