N-methylamide of o-phenoxyphenylthioglycolic acid

Base Information

Chemical Name:N-methylamide of o-phenoxyphenylthioglycolic acid
CAS No.:122993-04-8
Molecular Formula:C₁₅H₁₅NO₂S
Molecular Weight:273.356
Hs Code.:

Synonyms:

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Chemical Property of N-methylamide of o-phenoxyphenylthioglycolic acid

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Technology Process of N-methylamide of o-phenoxyphenylthioglycolic acid

There total 5 articles about N-methylamide of o-phenoxyphenylthioglycolic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107412-83-9
o-phenoxyphenylthioglycolic acid

: 122993-04-8
N-methylamide of o-phenoxyphenylthioglycolic acid

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 0.75 h / Heating

2: 2.0 g / H₂O / 1 h / Heating

With thionyl chloride; In water;

Reference yield:

: 55710-19-5
2-phenoxybenzenethiol

: 122993-04-8
N-methylamide of o-phenoxyphenylthioglycolic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 6 percent NaOH / 2.) water, heating, 1.5 h

2: thionyl chloride / 0.75 h / Heating

3: 2.0 g / H₂O / 1 h / Heating

With sodium hydroxide; thionyl chloride; In water;

Reference yield:

: Dithiocarbonic acid S-(2-phenoxy-phenyl) ester

: 122993-04-8
N-methylamide of o-phenoxyphenylthioglycolic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 39 g / Zn, 50 percent H₂SO₄ / 2 h / Heating

2: 1.) 6 percent NaOH / 2.) water, heating, 1.5 h

3: thionyl chloride / 0.75 h / Heating

4: 2.0 g / H₂O / 1 h / Heating

With sodium hydroxide; thionyl chloride; sulfuric acid; zinc; In water;