Technology Process of 2,4'-dibenzyloxy-2'-hydroxy-3',4,5,5',6'-pentamethoxychalcone
There total 1 articles about 2,4'-dibenzyloxy-2'-hydroxy-3',4,5,5',6'-pentamethoxychalcone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
2-methoxy-ethanol;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 640 mg / 30 percent H2O2, 20 percent NaOH / 2-methoxy-ethanol / 0.33 h / Ambient temperature
2: 70 mg / H2 / 10 percent Pd-C / ethyl acetate
With
sodium hydroxide; hydrogen; dihydrogen peroxide;
palladium on activated charcoal;
In
2-methoxy-ethanol; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 640 mg / 30 percent H2O2, 20 percent NaOH / 2-methoxy-ethanol / 0.33 h / Ambient temperature
2: 240 mg / K2CO3 / acetone / Heating
3: H2 / 10 percent Pd-C / ethyl acetate
4: BCl3 / CH2Cl2 / -50 °C
With
sodium hydroxide; hydrogen; dihydrogen peroxide; boron trichloride; potassium carbonate;
palladium on activated charcoal;
In
dichloromethane; 2-methoxy-ethanol; ethyl acetate; acetone;
