Pt(CF₃)[NC(C₆H₅)OCH₂CH₂][P(C₆H₅)3]2⁽¹⁺⁾*BF₄^(1-)=[Pt(CF₃)[NC(C₆H₅)OCH₂CH₂]P₂(C₆H₅)6]BF₄

Base Information

• Chemical Name: Pt(CF₃)[NC(C₆H₅)OCH₂CH₂][P(C₆H₅)3]2⁽¹⁺⁾*BF₄^(1-)=[Pt(CF₃)[NC(C₆H₅)OCH₂CH₂]P₂(C₆H₅)6]BF₄
• CAS No.: 154648-73-4
• Molecular Formula: BF₄*C₄₆H₃₉F₃NOP₂Pt
• Molecular Weight: 1022.65

Synonyms:

Chemical Property of Pt(CF₃)[NC(C₆H₅)OCH₂CH₂][P(C₆H₅)3]2⁽¹⁺⁾*BF₄^(1-)=[Pt(CF₃)[NC(C₆H₅)OCH₂CH₂]P₂(C₆H₅)6]BF₄

Chemical Property:

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Useful:

Technology Process of Pt(CF₃)[NC(C₆H₅)OCH₂CH₂][P(C₆H₅)3]2⁽¹⁺⁾*BF₄^(1-)=[Pt(CF₃)[NC(C₆H₅)OCH₂CH₂]P₂(C₆H₅)6]BF₄

There total 2 articles about Pt(CF₃)[NC(C₆H₅)OCH₂CH₂][P(C₆H₅)3]2⁽¹⁺⁾*BF₄^(1-)=[Pt(CF₃)[NC(C₆H₅)OCH₂CH₂]P₂(C₆H₅)6]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

Pt(CF3)(NCC6H5)[P(C6H5)3]2(1+)*BF4(1-)*0.5CH2Cl2=[Pt(CF3)(NCC6H5)P2(C6H5)6]BF4*0.5CH2Cl2 + 2-chloro-ethanol (107-07-3) → trans-bis(triphenylphosphino)Pt(CF3)Cl (71581-10-7) + Pt(CF3)[NC(C6H5)OCH2CH2][P(C6H5)3]2(1+)*BF4(1-)=[Pt(CF3)[NC(C6H5)OCH2CH2]P2(C6H5)6]BF4 (154648-73-4)

Guidance literature:

With n-C₄H₉Li; In tetrahydrofuran; hexane; Treating soln. of ClC2H4OH in THF (0°C) with n-BuLi (n-hexane) followed by Pt-compd., stirring of suspn. at 0°C for 20 min, and then reducing of volume.; Addn. of n-pentane, filtn., drying of soln., treating with Et2O. IR andGLC/MS spectra show presence of free oxazoline. Sepn. of Pt-compds. by taking advantage of the higher solubility of chloro complex in benzene. Elem. anal. of Pt-oxazoline compd.;

Reference yield:

trans-[Pt(CF3)(PPh3)2(Et2O)]BF4 → trans-bis(triphenylphosphino)Pt(CF3)Cl (71581-10-7) + Pt(CF3)[NC(C6H5)OCH2CH2][P(C6H5)3]2(1+)*BF4(1-)=[Pt(CF3)[NC(C6H5)OCH2CH2]P2(C6H5)6]BF4 (154648-73-4)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: n-C₄H₉Li / tetrahydrofuran; hexane

With n-C₄H₉Li; In tetrahydrofuran; hexane; dichloromethane;

upstream raw materials:

2-chloro-ethanol

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