Technology Process of C22H29NO6S
There total 4 articles about C22H29NO6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1: N-iodo-succinimide; water / dimethyl sulfoxide / 3.5 h / 20 °C
2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 100 °C
3: hydrogen; hydrogenchloride; 20% palladium hydroxide-activated charcoal / ethanol; 1,4-dioxane / 2 h
4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 20 °C
5: pyridine / tetrahydrofuran / 3 h / 0 - 20 °C
With
pyridine; hydrogenchloride; N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); 20% palladium hydroxide-activated charcoal; water; hydrogen; tri-n-butyl-tin hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dimethyl sulfoxide; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen; hydrogenchloride; 20% palladium hydroxide-activated charcoal / ethanol; 1,4-dioxane / 2 h
2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 20 °C
3: pyridine / tetrahydrofuran / 3 h / 0 - 20 °C
With
pyridine; hydrogenchloride; 20% palladium hydroxide-activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1,4-dioxane; ethanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 100 °C
2: hydrogen; hydrogenchloride; 20% palladium hydroxide-activated charcoal / ethanol; 1,4-dioxane / 2 h
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 20 °C
4: pyridine / tetrahydrofuran / 3 h / 0 - 20 °C
With
pyridine; hydrogenchloride; 2,2'-azobis(isobutyronitrile); 20% palladium hydroxide-activated charcoal; hydrogen; tri-n-butyl-tin hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; toluene;