o-methoxymethoxyphenyldibutylphosphine

Base Information

• Chemical Name: o-methoxymethoxyphenyldibutylphosphine
• CAS No.: 124629-82-9
• Molecular Formula: C₁₆H₂₇O₃P
• Molecular Weight: 298.362
• Mol file: 124629-82-9.mol

Synonyms:

Chemical Property of o-methoxymethoxyphenyldibutylphosphine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of o-methoxymethoxyphenyldibutylphosphine

There total 2 articles about o-methoxymethoxyphenyldibutylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenol (108-95-2,27073-41-2) → o-methoxymethoxyphenyldibutylphosphine (124629-82-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / NaOH, Bu₄NBr / benzene; H₂O / 4 h / Heating

2: 1) butyllithium / 1) a) hexane, THF, -5 deg C, b) -5 to 20 deg C, 2) 20-25 deg C

With sodium hydroxide; n-butyllithium; tetrabutylammomium bromide; In water; benzene;

DOI:10.1007/BF00953718

Reference yield:

dibutylphosphinic chloride (683-16-9) + O-methoxymethylphenol (824-91-9) → o-methoxymethoxyphenyldibutylphosphine (124629-82-9)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1) a) hexane, THF, -5 deg C, b) -5 to 20 deg C, 2) 20-25 deg C;

DOI:10.1007/BF00953718

Reference yield: 72.0%

o-methoxymethoxyphenyldibutylphosphine (124629-82-9) → o-dibutylphosphinoylphenol (124629-83-0)

Guidance literature:

With hydrogenchloride; In methanol; for 12h;

DOI:10.1007/BF00953718

upstream raw materials:

dibutylphosphinic chloride

O-methoxymethylphenol

phenol

Downstream raw materials:

o-dibutylphosphinoylphenol