MeCo(dmgH)(dpgH)Py

Base Information

• Chemical Name: MeCo(dmgH)(dpgH)Py
• CAS No.: 562104-15-8
• Molecular Formula: C₂₄H₂₆CoN₅O₄
• Molecular Weight: 507.495
• Mol file: 562104-15-8.mol

Synonyms:

Chemical Property of MeCo(dmgH)(dpgH)Py

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of MeCo(dmgH)(dpgH)Py

There total 1 articles about MeCo(dmgH)(dpgH)Py which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

trans-bis(dimethylglyoximato)(pyridine)chlorocobalt(III) + trans-bis(diphenylglyoximato)(pyridine)chlorocobalt(III) + methyl iodide (74-88-4) → trans-bis(dimethylglyoximato)(pyridine)methylcobalt(III) + trans-bis(diphenylglyoximato)(pyridine)methylcobalt(III) + MeCo(dmgH)(dpgH)Py (562104-15-8)

Guidance literature:

With NaOH; NaBH₄; In methanol; water; aq. soln. NaOH was added to suspn. ClCo(III)(dmgH)2Py and ClCo(III)(dpgH)2Py in MeOH and purged with Ar for 15 min, react. mixt was cooled to 0°C, NaBH4 in water and MeI in MeOH were added, react mixt. was stirred in the dark for 3 h; react. mixt. was poured in water, solid was filtered, dried, and chromed. on silica;

DOI:10.1021/om030089s

upstream raw materials:

methyl iodide