H2Ru3(CO)9(μ3-COMe)(CuPPh3)

Base Information

Chemical Name:H2Ru3(CO)9(μ3-COMe)(CuPPh3)
CAS No.:119503-10-5
Molecular Formula:C₂₉H₂₀CuO₁₀PRu₃
Molecular Weight:926.202
Hs Code.:

Synonyms:

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Chemical Property of H2Ru3(CO)9(μ3-COMe)(CuPPh3)

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Technology Process of H2Ru3(CO)9(μ3-COMe)(CuPPh3)

There total 1 articles about H2Ru3(CO)9(μ3-COMe)(CuPPh3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 22176-30-3
(triphenylphosphine)CuCl

: 119503-17-2
K{H2Ru3(CO)9(μ3-COMe)}

: 119503-16-1
H3Ru3(CO)7(PPh3)2(μ3-COMe)

: 119503-10-5
H2Ru3(CO)9(μ3-COMe)(CuPPh3)

: 119503-15-0
H3Ru3(CO)8PPh3(μ3-COMe)

Guidance literature:: In methanol; adding CuPPh3Cl to MeOH soln. of K(H2Ru3(CO)9(μ3-COMe)) (N2, room temp.), stirring (1 min), pptn.; monometallic Ru clusters formed in small yields in the filtrate; filtering, washing (MeOH); elem. anal.;

Reference yield:

: 119503-10-5
H2Ru3(CO)9(μ3-COMe)(CuPPh3)

: 119503-16-1
H3Ru3(CO)7(PPh3)2(μ3-COMe)

: 119503-15-0
H3Ru3(CO)8PPh3(μ3-COMe)

Guidance literature:: In dichloromethane; leaving soln. for several days;

Reference yield:

: 119503-10-5
H2Ru3(CO)9(μ3-COMe)(CuPPh3)

: 603-35-0
triphenylphosphine

: 119528-79-9
H2Ru3(CO)8(PPh3)(μ3-COMe)(CuPPh3)

Guidance literature:: In dichloromethane; refluxing H2Ru3(CO)9(μ3-COMe)(CuPPh3) and PPh3 in CH2Cl2 (N2, 30 min), cooling to room temp.; reducing vol., adding MeOH, pptn., washing (MeOH); elem. anal.;