(tetrakis(3,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzyl) 4,4',4'', 4'''-[[10-(2-[[3-(aminosulfonyl)phenyl]ethynyl]phenyl)porphyrin-5,15-diyl]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate^(2-))iron(II)

Base Information

• Chemical Name: (tetrakis(3,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzyl) 4,4',4'', 4'''-[[10-(2-[[3-(aminosulfonyl)phenyl]ethynyl]phenyl)porphyrin-5,15-diyl]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate^(2-))iron(II)
• CAS No.: 573658-64-7
• Molecular Formula: C₁₄₆H₁₈₉FeN₅O₄₆S
• Molecular Weight: 2838.03

Synonyms:

Chemical Property of (tetrakis(3,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzyl) 4,4',4'', 4'''-[[10-(2-[[3-(aminosulfonyl)phenyl]ethynyl]phenyl)porphyrin-5,15-diyl]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate^(2-))iron(II)

Chemical Property:

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Technology Process of (tetrakis(3,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzyl) 4,4',4'', 4'''-[[10-(2-[[3-(aminosulfonyl)phenyl]ethynyl]phenyl)porphyrin-5,15-diyl]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate^(2-))iron(II)

There total 1 articles about (tetrakis(3,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzyl) 4,4',4'', 4'''-[[10-(2-[[3-(aminosulfonyl)phenyl]ethynyl]phenyl)porphyrin-5,15-diyl]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate^(2-))iron(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis(3,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzyl) 4,4',4'', 4'''-[[10-(2-[[3-(aminosulfonyl)phenyl]ethynyl]phenyl)porphyrin-5,15-diyl]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate + iron(II) bromide (7789-46-0) → (tetrakis(3,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzyl) 4,4',4'', 4'''-[[10-(2-[[3-(aminosulfonyl)phenyl]ethynyl]phenyl)porphyrin-5,15-diyl]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate(2-))iron(II) (573658-64-7)

Guidance literature:

With 2,6-dimethylpyridine; In tetrahydrofuran; (N2); FeBr2 and 2,6-lutidine added to a soln. of ligand, stirred at 20°C; evapd. (vac.), chromd. (neutral Al2O3, abs. THF/abs. MeOH); used as a soln. in abs. toluene;

DOI:10.1002/hlca.200490288

Reference yield: 99.0%

1,2-dimethyl-1H-imidazole (1739-84-0) + (tetrakis(3,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzyl) 4,4',4'', 4'''-[[10-(2-[[3-(aminosulfonyl)phenyl]ethynyl]phenyl)porphyrin-5,15-diyl]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate(2-))iron(II) (573658-64-7) → (tetrakis(3,5-bis[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]benzyl) 4,4',4'', 4'''-[[10-(2-[[3-(aminosulfonyl)phenyl]ethynyl]phenyl)porphyrin-5,15-diyl]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate(2-))(1,2-dimethyl-1H-imidazole)iron(II)

Guidance literature:

In toluene; (N2); not isolated, detected by UV-vis;

DOI:10.1002/hlca.200490288

upstream raw materials:

iron(II) bromide

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