homo-ent-galbanic acid

Base Information

Chemical Name:homo-ent-galbanic acid
CAS No.:1206911-01-4
Molecular Formula:C₂₅H₃₂O₅
Molecular Weight:412.526
Hs Code.:

Synonyms:

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Chemical Property of homo-ent-galbanic acid

Chemical Property:

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Technology Process of homo-ent-galbanic acid

There total 7 articles about homo-ent-galbanic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₂O₄

: 1206911-01-4
homo-ent-galbanic acid

Guidance literature:: With sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 25 ℃; for 12h;
DOI:10.1002/ejoc.200901021

Reference yield:

: 1035948-08-3
C₁₆H₂₈O

: 1206911-01-4
homo-ent-galbanic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: tert-butyldimethylsilyl chloride

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3 h / 25 °C / Inert atmosphere

2.2: 1 h / 25 °C / Inert atmosphere

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 12 h / 25 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 25 °C

5.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -60 °C / Inert atmosphere

6.1: sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 25 °C

With sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; tert-butyldimethylsilyl chloride; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 3.1: Mitsunobu reaction / 5.1: Swern oxidation;
DOI:10.1002/ejoc.200901021

Reference yield:

: 1035948-05-0
C₁₆H₂₈O₃

: 1206911-01-4
homo-ent-galbanic acid

Guidance literature:: Multi-step reaction with 9 steps

1.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -60 °C / Inert atmosphere

2.1: potassium tert-butylate / toluene / 0.75 h / 20 °C / Inert atmosphere; Cooling with ice

3.1: lithium aluminium tetrahydride

4.1: tert-butyldimethylsilyl chloride

5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3 h / 25 °C / Inert atmosphere

5.2: 1 h / 25 °C / Inert atmosphere

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 12 h / 25 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 25 °C

8.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -60 °C / Inert atmosphere

9.1: sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 25 °C

With sodium chlorite; potassium dihydrogenphosphate; lithium aluminium tetrahydride; 2-methyl-but-2-ene; oxalyl dichloride; di-isopropyl azodicarboxylate; potassium tert-butylate; tetrabutyl ammonium fluoride; tert-butyldimethylsilyl chloride; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; toluene; tert-butyl alcohol; 1.1: Swern oxidation / 2.1: Wittig reaction / 6.1: Mitsunobu reaction / 8.1: Swern oxidation;
DOI:10.1002/ejoc.200901021