[Ru(CO)(η-C2H4)Cl2(PMe2Ph)2]

Base Information

Chemical Name:[Ru(CO)(η-C2H4)Cl2(PMe2Ph)2]
CAS No.:60595-73-5
Molecular Formula:C₁₉H₂₆Cl₂OP₂Ru
Molecular Weight:504.338
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ru(CO)(η-C2H4)Cl2(PMe2Ph)2]

Chemical Property:

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Technology Process of [Ru(CO)(η-C2H4)Cl2(PMe2Ph)2]

There total 1 articles about [Ru(CO)(η-C2H4)Cl2(PMe2Ph)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 17141-01-4,17141-04-7,25165-53-1,60426-65-5
all-trans-[Ru(CO)2(PMe₂Ph)Cl₂]

: 74-85-1
ethene

: 60595-73-5,67225-39-2
[Ru(CO)(η-C2H4)Cl2(PMe2Ph)2]

Guidance literature:: In chloroform; bubbling C2H4 through soln. of Ru-complex (313 K, 72 h); solvent removal (reduced pressure), recrystn. (Me2CO/light petroleum satd. with C2H4); elem. anal.;
DOI:10.1039/DT9760000953

Reference yield: 92.0%

: 60595-73-5,67225-39-2
[Ru(CO)(η-C2H4)Cl2(PMe2Ph)2]

: sodium perchlorate

: 672-66-2
Dimethyl(phenyl)phosphine

: 80411-21-8
[Ru(CO)(CH₂CH₂PMe₂Ph)Cl(PMe₂Ph)3][ClO₄]

Guidance literature:: In acetone; byproducts: NaCl; 273 K, 24 h, under dry N2; filtration of NaCl, addn. of light petroleum, slow evapn. under N2 stream; elem.anal.;
DOI:10.1039/DT9810002112

Reference yield:

: 75-18-3
dimethylsulfide

: 60595-73-5,67225-39-2
[Ru(CO)(η-C2H4)Cl2(PMe2Ph)2]

: 60595-71-3
[Ru(CO)Cl₂(PMe₂Ph)2(SMe₂)]

Guidance literature:: In chloroform-d1; under dry N2, 1 week at 268 K, 1 week at 273 K, 1 week at 278 K; evapn. in vac., crystn. from ethanol, washing with light petroleum, drying in vac.;
DOI:10.1039/DT9810002112