(S)-2,6,6-Trimethyl-1-(3-methyl-pent-4-enyl)-cyclohexa-2,4-dienol

Base Information

Chemical Name:(S)-2,6,6-Trimethyl-1-(3-methyl-pent-4-enyl)-cyclohexa-2,4-dienol
CAS No.:54702-01-1
Molecular Formula:C₁₅H₂₄O
Molecular Weight:220.355
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2,6,6-Trimethyl-1-(3-methyl-pent-4-enyl)-cyclohexa-2,4-dienol

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Technology Process of (S)-2,6,6-Trimethyl-1-(3-methyl-pent-4-enyl)-cyclohexa-2,4-dienol

There total 5 articles about (S)-2,6,6-Trimethyl-1-(3-methyl-pent-4-enyl)-cyclohexa-2,4-dienol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2436-90-0
(S)-(+)-dihydromyrcene

: 54702-01-1,54702-02-2,59822-11-6,59822-14-9,79897-85-1,79897-86-2,79897-90-8,79951-68-1
(S)-2,6,6-Trimethyl-1-(3-methyl-pent-4-enyl)-cyclohexa-2,4-dienol

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / 40percent peracetic acid, sodium acetate / CH₂Cl₂; H₂O / 2 h / 20 °C

2: 63 percent / LiClO₄ / petroleum ether / 5 h / Heating

3: 1) potassium t-butoxide, oxygen, 2) LiAlH₄ / 1) glyme, 90 min, 2) ether, reflux, 8 h

4: phosphorous tribromide, pyridine / 3 h / 25 °C

5: 1) lithium (cont. 1.5percent natrium) / diethyl ether

With pyridine; peracetic acid; lithium aluminium tetrahydride; lithium (cont. 1.5percent natrium); potassium tert-butylate; oxygen; sodium acetate; lithium perchlorate; phosphorus tribromide; In diethyl ether; dichloromethane; water; Petroleum ether;
DOI:10.1002/hlca.19810640515

Reference yield:

: 75420-45-0,54702-04-4
(S)-(+)-3-methyl-4-penten-1-ol

: 54702-01-1,54702-02-2,59822-11-6,59822-14-9,79897-85-1,79897-86-2,79897-90-8,79951-68-1
(S)-2,6,6-Trimethyl-1-(3-methyl-pent-4-enyl)-cyclohexa-2,4-dienol

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorous tribromide, pyridine / 3 h / 25 °C

2: 1) lithium (cont. 1.5percent natrium) / diethyl ether

With pyridine; lithium (cont. 1.5percent natrium); phosphorus tribromide; In diethyl ether;
DOI:10.1002/hlca.19810640515

Reference yield:

: 502164-45-6
2,2-dimethyl-3-((S)-3-methylpent-4-enyl)oxirane

: 54702-01-1,54702-02-2,59822-11-6,59822-14-9,79897-85-1,79897-86-2,79897-90-8,79951-68-1
(S)-2,6,6-Trimethyl-1-(3-methyl-pent-4-enyl)-cyclohexa-2,4-dienol

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / LiClO₄ / petroleum ether / 5 h / Heating

2: 1) potassium t-butoxide, oxygen, 2) LiAlH₄ / 1) glyme, 90 min, 2) ether, reflux, 8 h

3: phosphorous tribromide, pyridine / 3 h / 25 °C

4: 1) lithium (cont. 1.5percent natrium) / diethyl ether

With pyridine; lithium aluminium tetrahydride; lithium (cont. 1.5percent natrium); potassium tert-butylate; oxygen; lithium perchlorate; phosphorus tribromide; In diethyl ether; Petroleum ether;
DOI:10.1002/hlca.19810640515