D-arabino-[2]hexosulose bis-benzoylhydrazone

Base Information

• Chemical Name: D-arabino-[2]hexosulose bis-benzoylhydrazone
• CAS No.: 13032-73-0
• Molecular Formula: C₂₀H₂₂N₄O₆
• Molecular Weight: 414.418
• Mol file: 13032-73-0.mol

Synonyms:

Chemical Property of D-arabino-[2]hexosulose bis-benzoylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of D-arabino-[2]hexosulose bis-benzoylhydrazone

There total 2 articles about D-arabino-[2]hexosulose bis-benzoylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-glucosone (643-71-0,25990-59-4,26187-86-0,26345-59-5,49865-02-3,54142-77-7,81844-97-5,81844-98-6,81845-00-3,89576-70-5,90457-64-0,1854-25-7) + benzoic acid hydrazide (613-94-5) → D-arabino-[2]hexosulose bis-benzoylhydrazone (13032-73-0)

Guidance literature:

DOI:10.1016/S0008-6215(00)81484-6

Reference yield:

→ D-arabino-[2]hexosulose bis-benzoylhydrazone (13032-73-0)

Guidance literature:

DOI:10.1039/j39670000519

Reference yield:

D-arabino-[2]hexosulose bis-benzoylhydrazone (13032-73-0) → D-arabino-Hexosulose-benzoylhydrazon-(1)

Guidance literature:

Multi-step reaction with 2 steps

1: CuSO₄

2: methanol

With copper(II) sulfate; In methanol;

DOI:10.1039/j39680001465

upstream raw materials:

D-glucosone

benzoic acid hydrazide

Downstream raw materials:

D-glucosone

3,4,5,6-Tetra-O-acetyl-D-arabino-hexosulose-bis-(benzoylhydrazon)

D-Arabino-hexosulose-bis-(4-brom-benzoyl-hydrazon)

D-Arabino-hexosulose-bis-(4-iod-benzoyl-hydrazon)