N-isopropyl-N-phenylperimidinium iodide

Base Information

Chemical Name:N-isopropyl-N-phenylperimidinium iodide
CAS No.:1245928-36-2
Molecular Formula:C₂₀H₁₉N₂*I
Molecular Weight:414.289
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-isopropyl-N-phenylperimidinium iodide

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Technology Process of N-isopropyl-N-phenylperimidinium iodide

There total 1 articles about N-isopropyl-N-phenylperimidinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 75-30-9
2-iodo-propane

: 62206-31-9
1-phenylperimidine

: 1245928-36-2
N-isopropyl-N-phenylperimidinium iodide

Guidance literature:: for 48h; Reflux; Darkness;
DOI:10.1021/om100604u

Reference yield: 60.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 1245928-36-2
N-isopropyl-N-phenylperimidinium iodide

: [Ir(iodo)(1,5-cyclooctadiene)(N-isopropyl-N-phenylperimidine)]

Guidance literature:: With LiN(SiMe₃)2; In tetrahydrofuran; byproducts: LiI; (Ar); using Schlenk techniques; addn. of THF to LiN(SiMe3)2 (excess), (Ir(COD)Cl)2 and N-isopropyl-N-phenylperimidinium iodide (excess) at room temp., stirring for 6 h at room temp.; evapn. of solvent, extn. with CH2Cl2, flash chromy. on silica gel using CH2Cl2 at the eluent; elem. anal.;
DOI:10.1021/om100604u