Sn(C₆H₃(C₆H₂(CH₃)3)2)2(OH)2

Base Information

• Chemical Name: Sn(C₆H₃(C₆H₂(CH₃)3)2)2(OH)2
• CAS No.: 386768-34-9
• Molecular Formula: C₄₈H₅₂O₂Sn
• Molecular Weight: 779.65
• Mol file: 386768-34-9.mol

Synonyms:

Chemical Property of Sn(C₆H₃(C₆H₂(CH₃)3)2)2(OH)2

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Sn(C₆H₃(C₆H₂(CH₃)3)2)2(OH)2

There total 2 articles about Sn(C₆H₃(C₆H₂(CH₃)3)2)2(OH)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

Sn(C6H3-2,6-(C6H2-2,4,6-(CH3)3)2)2 (188685-27-0) + dinitrogen monoxide (10024-97-2) → Sn(C6H3(C6H2(CH3)3)2)2(OH)2 (386768-34-9)

Guidance literature:

In toluene; a soln. of Sn-compound in toluene was treated with N2O gas at room temp., the soln. was stirred for 16 h (N2); toluene was removed, the residue was extd. with hexane, decanted, reduced in vol., stored at -20°C for 30 h;

DOI:10.1021/om010548u

Reference yield: 37.2%

trimethylamine-N-oxide (1184-78-7) + Sn(C6H3-2,6-(C6H2-2,4,6-(CH3)3)2)2 (188685-27-0) → Sn(C6H3(C6H2(CH3)3)2)2(OH)2 (386768-34-9)

Guidance literature:

In diethyl ether; a soln. of Sn-compound in diethyl ether was added to Me3NO in ether at 25°C with rapid stirring, the mixt. was stirred for 16 h (N2); filtered, concd., stored at -20°C for 30 h;

DOI:10.1021/om010548u

upstream raw materials:

trimethylamine-N-oxide

Sn(C₆H₃-2,6-(C₆H₂-2,4,6-(CH₃)₃)₂)₂

dinitrogen monoxide