(C₅(CH₃)5)IrCl₂(P(C₆H₅)2C₂C₆H₅)

Base Information

Chemical Name:(C₅(CH₃)5)IrCl₂(P(C₆H₅)2C₂C₆H₅)
CAS No.:439293-40-0
Molecular Formula:C₃₀H₃₀Cl₂IrP
Molecular Weight:684.668
Hs Code.:

(C<sub>5</sub>(CH<sub>3</sub>)5)IrCl<sub>2</sub>(P(C<sub>6</sub>H<sub>5</sub>)2C<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₅(CH₃)5)IrCl₂(P(C₆H₅)2C₂C₆H₅)

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Technology Process of (C₅(CH₃)5)IrCl₂(P(C₆H₅)2C₂C₆H₅)

There total 1 articles about (C₅(CH₃)5)IrCl₂(P(C₆H₅)2C₂C₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 7608-17-5
2-diphenylphosphino-1-phenylethyne

: bis((μ-chloro)chloro(pentamethylcyclopentadienyl)iridium)

: 439293-40-0
(C₅(CH₃)5)IrCl₂(P(C₆H₅)2C₂C₆H₅)

Guidance literature:: In acetone; ligand was added to suspn. of Ir-complex in acetone, stirred for 5 min under Ar; evapd. to dryness, treated with Et2O; elem. anal.;
DOI:10.1021/om020052s

Reference yield: 48.0%

: 439293-40-0
(C₅(CH₃)5)IrCl₂(P(C₆H₅)2C₂C₆H₅)

: 2923-28-6
silver trifluoromethanesulfonate

: 439293-44-4
(C₅(CH₃)5)IrCl(P(C₆H₅)2C₂C₆H₅)2⁽¹⁺⁾*CF₃SO₃^(1-)=Ir(C₅(CH₃)5)Cl(P(C₆H₅)2C₂C₆H₅)2CF₃SO₃

Guidance literature:: In acetone; byproducts: AgCl; soln. of Ir-complex in acetone was treated with AgCF3SO3, stirred at room temp. for 3 h in the absence of light, filtered, treated with ligand for 30 min under Ar; concd. in vacuo, treated with Et2O, stored for 2 h at -40°C, filtered, washed with Et2O; elem. anal.;
DOI:10.1021/om020052s

Reference yield:

: cis-[(pentafluorophenyl)2 (tetrahydrofurane)2 platinum(II)]

: 439293-40-0
(C₅(CH₃)5)IrCl₂(P(C₆H₅)2C₂C₆H₅)

: 439293-47-7,439293-53-5
[(η5-Cp*)Ir(μ-Cl)2(PPh2C2Ph)Pt(C6F5)2]

: 439293-53-5,439293-47-7
[Cp*ClIr(μ-Cl)(μ-PPh2C2Ph)Pt(C6F5)2]

Guidance literature:: In dichloromethane; Pt-complex was added to soln. of Ir-complex in CH2Cl2, stirred for 20 min under Ar; solvent was evap. in vacuo, filtered, washed with Et2O; elem. anal.;
DOI:10.1021/om020052s