C₂₂H₄₂O₂Si₂

Base Information

Chemical Name:C₂₂H₄₂O₂Si₂
CAS No.:1257333-83-7
Molecular Formula:C₂₂H₄₂O₂Si₂
Molecular Weight:394.745
Hs Code.:

C<sub>22</sub>H<sub>42</sub>O<sub>2</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₂₂H₄₂O₂Si₂

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Technology Process of C₂₂H₄₂O₂Si₂

There total 4 articles about C₂₂H₄₂O₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63314-77-2
α-propyl-2-hydroxybenzylalcohol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1257333-83-7
C₂₂H₄₂O₂Si₂

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 17h;
DOI:10.1021/ja1086547

Reference yield:

: 1257333-57-5
C₁₄H₂₂OSi

: 1257333-83-7
C₂₂H₄₂O₂Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; potassium hydrogencarbonate / tetrahydrofuran; methanol; water / 40 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 17 h / 20 °C

With 1H-imidazole; dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; 1: Tamao-Fleming oxidation;
DOI:10.1021/ja1086547

Reference yield:

: 1257333-98-4
C₁₄H₂₄OSi

: 1257333-83-7
C₂₂H₄₂O₂Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: norborn-2-ene; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 1,10-Phenanthroline / tetrahydrofuran / 17 h / 100 °C / Inert atmosphere

2: dihydrogen peroxide; potassium hydrogencarbonate / tetrahydrofuran; methanol; water / 40 °C

3: 1H-imidazole / N,N-dimethyl-formamide / 17 h / 20 °C

With 1H-imidazole; norborn-2-ene; 1,10-Phenanthroline; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; 2: Tamao-Fleming oxidation;
DOI:10.1021/ja1086547