[Pd((2,6-(i-Pr)2C₆H₃)-N=CMeCMe=N-(2,6-(i-Pr)2C₆H₃))Me(acrylonitrile)][B(3,5-(CF₃)2C₆H₃)4]

Base Information

• Chemical Name: [Pd((2,6-(i-Pr)2C₆H₃)-N=CMeCMe=N-(2,6-(i-Pr)2C₆H₃))Me(acrylonitrile)][B(3,5-(CF₃)2C₆H₃)4]
• CAS No.: 867065-04-1
• Molecular Formula: C₃₂H₁₂BF₂₄*C₃₂H₄₆N₃Pd
• Molecular Weight: 1442.38

Synonyms:

Chemical Property of [Pd((2,6-(i-Pr)2C₆H₃)-N=CMeCMe=N-(2,6-(i-Pr)2C₆H₃))Me(acrylonitrile)][B(3,5-(CF₃)2C₆H₃)4]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Pd((2,6-(i-Pr)2C₆H₃)-N=CMeCMe=N-(2,6-(i-Pr)2C₆H₃))Me(acrylonitrile)][B(3,5-(CF₃)2C₆H₃)4]

There total 1 articles about [Pd((2,6-(i-Pr)2C₆H₃)-N=CMeCMe=N-(2,6-(i-Pr)2C₆H₃))Me(acrylonitrile)][B(3,5-(CF₃)2C₆H₃)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[[(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]PdMe(OEt2)]B[3,5-(CF3)2C6H3]4 + acrylonitrile (107-13-1,25014-41-9) → [Pd((2,6-(i-Pr)2C6H3)-N=CMeCMe=N-(2,6-(i-Pr)2C6H3))Me(acrylonitrile)][B(3,5-(CF3)2C6H3)4] (867065-04-1)

Guidance literature:

In further solvent(s); under purified Ar using Schlenk line techniques; soln. of Pd complex in acrylonitrile stirred for 1 h; acrylonitrile removed; dark orange/brown oil washed with hexanes and dried under reduced pressure; yellow solid washed by repeated extns. with hexanes and dried overnight under reduced pressure; elem. anal.;

DOI:10.1016/j.jorganchem.2005.07.031

Reference yield:

[Pd((2,6-(i-Pr)2C6H3)-N=CMeCMe=N-(2,6-(i-Pr)2C6H3))Me(acrylonitrile)][B(3,5-(CF3)2C6H3)4] (867065-04-1) + acrylonitrile (107-13-1,25014-41-9) → [Pd(2,6-(i-Pr)2C6H3)N=CMeCMe=N-(2,6-(i-Pr)2C6H3))Me(Et2O)](1+) (867065-05-2)

Guidance literature:

In further solvent(s); Pd complex dissolved in acrylonitrile; soln. stirred under Ar at room temp. for 12 hs or at 50°C for 2 hs; acrylonitrile removed (vac.); washed (hexane); monitored by NMR and massspectroscopy;

DOI:10.1016/j.jorganchem.2005.07.031

Reference yield:

[Pd((2,6-(i-Pr)2C6H3)-N=CMeCMe=N-(2,6-(i-Pr)2C6H3))Me(acrylonitrile)][B(3,5-(CF3)2C6H3)4] (867065-04-1) + acrylonitrile (107-13-1,25014-41-9) → [Pd(2,6-(i-Pr)2C6H3)N=CMeCMe=N-(2,6-(i-Pr)2C6H3)(CH(CN)C2H5)]2(2+)

Guidance literature:

In further solvent(s); Pd complex dissolved in acrylonitrile; soln. refluxed under Ar at 77°C for 12 hs; acrylonitrile removed (vac.); washed (hexane); monitored by NMR and massspectroscopy;

DOI:10.1016/j.jorganchem.2005.07.031

upstream raw materials:

acrylonitrile

Downstream raw materials:

[Pd(2,6-(i-Pr)2C₆H₃)N=CMeCMe=N-(2,6-(i-Pr)2C₆H₃))Me(Et₂O)]⁽¹⁺⁾

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