(+/-)-1,2,4,5-Tetra-O-benzyl-myo-inositol 3,6-bis

Base Information

Chemical Name:(+/-)-1,2,4,5-Tetra-O-benzyl-myo-inositol 3,6-bis
CAS No.:140887-15-6
Molecular Formula:C₄₆H₅₀N₄O₁₂P₂
Molecular Weight:912.87
Hs Code.:

(+/-)-1,2,4,5-Tetra-O-benzyl-myo-inositol 3,6-bis<di(2-cyanoethyl) phosphate>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-1,2,4,5-Tetra-O-benzyl-myo-inositol 3,6-bis

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (+/-)-1,2,4,5-Tetra-O-benzyl-myo-inositol 3,6-bis

There total 13 articles about (+/-)-1,2,4,5-Tetra-O-benzyl-myo-inositol 3,6-bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: Phosphorous acid bis-(2-cyano-ethyl) ester (1R,2S,3R,4R,5R,6R)-2,3,5,6-tetrakis-benzyloxy-4-[bis-(2-cyano-ethoxy)-phosphanyloxy]-cyclohexyl ester

: 140887-15-6
(+/-)-1,2,4,5-Tetra-O-benzyl-myo-inositol 3,6-bis

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid;
DOI:10.1016/S0008-6215(00)90497-X

Reference yield:

: 100-39-0
benzyl bromide

: 140887-15-6
(+/-)-1,2,4,5-Tetra-O-benzyl-myo-inositol 3,6-bis

Guidance literature:: Multi-step reaction with 5 steps

1: NaH / dimethylformamide

2: K-tert-butoxide / dimethylsulfoxide

3: HCl / acetone / 0.5 h / Heating

5: 59 percent / m-chloroperoxybenzoic acid

With hydrogenchloride; potassium tert-butylate; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0008-6215(00)90497-X

Reference yield:

: 98906-30-0,104873-76-9,111466-07-0,114297-88-0,114297-91-5,114419-08-8,115184-71-9,115509-75-6,115509-76-7,118354-54-4,118354-55-5,128163-34-8,129706-80-5,136521-84-1,149713-88-2,149713-95-1
(+/-)-2,5,6-tri-O-benzyl-myo-inositol

: 140887-15-6
(+/-)-1,2,4,5-Tetra-O-benzyl-myo-inositol 3,6-bis

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / toluene p-sulphonic acid / acetone / 5 h / 20 °C

2: NaH / dimethylformamide

3: 1.19 g / 1M HCl / acetone; methanol / 1 h / 20 °C

4: 76 percent / dibutyltin oxide, tetrabutylammonium bromide / acetonitrile / 20 h / Heating

5: dichlorodicyanobenzoquinone / CH₂Cl₂; H₂O / 20 °C

7: 59 percent / m-chloroperoxybenzoic acid

With hydrogenchloride; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/S0008-6215(00)90497-X