[(κN1:κN2-2,6-bis((1,3-di-tert-butylimidazolyn-2-imino)methyl)pyridine)Cu(2,6-o-XyNC))]PF6

Base Information

• Chemical Name: [(κN1:κN2-2,6-bis((1,3-di-tert-butylimidazolyn-2-imino)methyl)pyridine)Cu(2,6-o-XyNC))]PF6
• CAS No.: 946829-10-3
• Molecular Formula: C₃₈H₅₆CuN₈*F₆P
• Molecular Weight: 833.426
• Mol file: 946829-10-3.mol

Synonyms:

Chemical Property of [(κN1:κN2-2,6-bis((1,3-di-tert-butylimidazolyn-2-imino)methyl)pyridine)Cu(2,6-o-XyNC))]PF6

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(κN1:κN2-2,6-bis((1,3-di-tert-butylimidazolyn-2-imino)methyl)pyridine)Cu(2,6-o-XyNC))]PF6

There total 1 articles about [(κN1:κN2-2,6-bis((1,3-di-tert-butylimidazolyn-2-imino)methyl)pyridine)Cu(2,6-o-XyNC))]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2,6-bis[(1,3-di-tert-butylimidazolyn-2-imino)methyl]pyridine (946828-70-2) + tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + 2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) → [(κN1:κN2-2,6-bis((1,3-di-tert-butylimidazolyn-2-imino)methyl)pyridine)Cu(2,6-o-XyNC))]PF6 (946829-10-3)

Guidance literature:

In tetrahydrofuran; addn. of soln. of bis(imidazolin-2-imine) ligand in THF to a soln. of Cu(MeCN)4PF6 in THF under Ar at room temp., addn. of (CH3)2C6H3NC, stirring for 1 h; removal of solvent, washing with hexane, elem. anal.;

DOI:10.1039/b703183a

upstream raw materials:

2,6-bis[(1,3-di-tert-butylimidazolyn-2-imino)methyl]pyridine

tetrakis(actonitrile)copper(I) hexafluorophosphate

2,6-dimethylphenyl isonitrile