C₂₆H₂₄Br₂N₂O₃

Base Information

Chemical Name:C₂₆H₂₄Br₂N₂O₃
CAS No.:1307893-39-5
Molecular Formula:C₂₆H₂₄Br₂N₂O₃
Molecular Weight:572.296
Hs Code.:

C<sub>26</sub>H<sub>24</sub>Br<sub>2</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₆H₂₄Br₂N₂O₃

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Technology Process of C₂₆H₂₄Br₂N₂O₃

There total 10 articles about C₂₆H₂₄Br₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1307893-43-1
C₁₉H₂₁BrN₂O₂

: 586-75-4
4-chlorobenzoyl chloride

: 1307893-39-5
C₂₆H₂₄Br₂N₂O₃

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 14h;
DOI:10.1055/s-0030-1259324

Reference yield:

: 106-40-1
4-bromo-aniline

: 1307893-39-5
C₂₆H₂₄Br₂N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydride / tetrahydrofuran / 0.5 h / 20 °C

1.2: 0.5 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / 20 °C

3.1: triethylamine / dichloromethane / 14 h / 20 °C

With lithium aluminium tetrahydride; potassium hydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0030-1259324

Reference yield:

: 1738-78-9
L-phenylalanine benzyl ester p-toluene-sulfonic acid salt

: 1307893-39-5
C₂₆H₂₄Br₂N₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 5 h / 20 °C

2.1: dmap / acetonitrile / 0.5 h / 20 °C

3.1: potassium hexamethylsilazane / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / -60 °C

4.1: potassium hydride / tetrahydrofuran / 0.5 h / 20 °C

4.2: 0.5 h / 20 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / 20 °C

6.1: triethylamine / dichloromethane / 14 h / 20 °C

With dmap; lithium aluminium tetrahydride; potassium hydride; potassium hexamethylsilazane; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1055/s-0030-1259324