dichloro(2-methoxyphenyl)phenylsilane

Base Information

Chemical Name:dichloro(2-methoxyphenyl)phenylsilane
CAS No.:53864-05-4
Molecular Formula:C₁₃H₁₂Cl₂OSi
Molecular Weight:283.229
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dichloro(2-methoxyphenyl)phenylsilane

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Technology Process of dichloro(2-methoxyphenyl)phenylsilane

There total 1 articles about dichloro(2-methoxyphenyl)phenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 578-57-4
2-bromoanisole

: 98-13-5
Phenyltrichlorosilane

: 53864-05-4
dichloro(2-methoxyphenyl)phenylsilane

Guidance literature:: 2-bromoanisole; With n-butyllithium; Inert atmosphere;

Phenyltrichlorosilane; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1002/anie.201105636

Reference yield: 32.0%

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 53864-05-4
dichloro(2-methoxyphenyl)phenylsilane

: 445494-25-7
Ph(2-MeOC₆H₄)ClSiFe(CO)2(C₅H₅)]

Guidance literature:: With Na; In tetrahydrofuran; diethyl ether; byproducts: NaCl; (N2); standard Schlenk technique; Fe complex in THF was reduced with Na amalgam; soln. was transferred into Schlenk flask with Ph(2-MeOC6H4)SiCl2 in ether at 0°C; stirred soln. was warmed to room temp.; solvent removed (vac.); ether added; soln. passed through filter stick; solvent removed; chromd. (SiO2, CH2Cl2/petroleum spirit, 1/5); recrystd.(ether/petroleum spirit); elem. anal.;
DOI:10.1016/S0022-328X(01)01403-6