Mercury, chloro[2-(2-pyridinyl)phenyl]-

Base Information

Chemical Name:Mercury, chloro[2-(2-pyridinyl)phenyl]-
CAS No.:106995-39-5
Molecular Formula:C11H8ClHgN
Molecular Weight:390.234
Hs Code.:
DSSTox Substance ID:DTXSID30457821

Synonyms:Mercury, chloro[2-(2-pyridinyl)phenyl]-;106995-39-5;DTXSID30457821;[2-(pyridin-2-yl)phenyl]mercury(ii) chloride

Suppliers and Price of Mercury, chloro[2-(2-pyridinyl)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Mercury, chloro[2-(2-pyridinyl)phenyl]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:391.005171
Heavy Atom Count:14
Complexity:177

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C2=CC=CC=N2)[Hg]Cl

Technology Process of Mercury, chloro[2-(2-pyridinyl)phenyl]-

There total 3 articles about Mercury, chloro[2-(2-pyridinyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.5%

: 1008-89-5
2-phenylpyridine

: 1600-27-7
mercury(II) diacetate

: 106995-39-5
2-(2'-pyridyl)phenylmercury(II) chloride

Guidance literature:: With lithium chloride; In ethanol; 2-phenylpyridine and Hg(CH3COO)2 in absolute EtOH were refluxed for 24 h, LiCl in absolute EtOH was added, mixture heated for 15 min; poured into distd. water, filtered, crystn. at room temp., washed with cold MeOH, dried at 60°C, elem. anal.;;

Reference yield:

: 1008-89-5
2-phenylpyridine

: 106995-39-5
2-(2'-pyridyl)phenylmercury(II) chloride

Guidance literature:: 2-phenylpyridine; With mercury(II) diacetate; In ethanol; for 12h; Reflux;

With lithium chloride; In methanol; ethanol; for 1h; Reflux;
DOI:10.1002/adsc.201300005

Reference yield:

: 1008-89-5
2-phenylpyridine

: 1600-27-7
mercury(II) diacetate

: lithium chloride

: 106995-39-5
2-(2'-pyridyl)phenylmercury(II) chloride

Guidance literature:: In methanol; ethanol; soln. of pyridine derivative in EtOH was added slowly to stirred soln. of Hg(OAc)2 in EtOH, mixt. was heated under reflux for 12 h, filtered into soln. of LiCl in MeOH, mixt. was heated under reflux for 1 h, allowed to cool overnight; ppt. filtered off, washed with H2O and EtOH at 0°C, recrystd. from CH2Cl2; elem. anal.;
DOI:10.1016/S0022-328X(99)00645-2