N⁵-Benzoyl-5-amino-3-methyl-1-(phenylsulfonyl)indole

Base Information

Chemical Name:N⁵-Benzoyl-5-amino-3-methyl-1-(phenylsulfonyl)indole
CAS No.:124400-53-9
Molecular Formula:C₂₂H₁₈N₂O₃S
Molecular Weight:390.463
Hs Code.:

N<sup>5</sup>-Benzoyl-5-amino-3-methyl-1-(phenylsulfonyl)indole

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁵-Benzoyl-5-amino-3-methyl-1-(phenylsulfonyl)indole

Chemical Property:

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Technology Process of N⁵-Benzoyl-5-amino-3-methyl-1-(phenylsulfonyl)indole

There total 5 articles about N⁵-Benzoyl-5-amino-3-methyl-1-(phenylsulfonyl)indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3393-96-2
p-nitrobenzanilide

: 124400-53-9
N⁵-Benzoyl-5-amino-3-methyl-1-(phenylsulfonyl)indole

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / H₂ / 10percent Pd/C / ethyl acetate / 2 h / 25 °C / 2585.7 Torr

2: 84 percent / pyridine / tetrahydrofuran / 8 h / Heating

3: 79 percent / lead tetraacetate / CHCl₃ / 12 h / 25 °C

4: 54 percent / BF₃*Et₂O / CH₂Cl₂ / 1) -78 deg C, 12 h, 2) -20 deg C, 12 h

5: 1) OsO₄, NaIO₄, 2) H₂SO₄ (10percent in CH₂Cl₂) / 1) acetone, water, 25 deg C, 2) CH₂Cl₂, 25 deg C

With pyridine; lead(IV) acetate; sodium periodate; osmium(VIII) oxide; sulfuric acid; boron trifluoride diethyl etherate; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; chloroform; ethyl acetate;
DOI:10.1021/jo00291a059

Reference yield:

: 17625-83-1
N-(4-aminophenyl)benzamide

: 124400-53-9
N⁵-Benzoyl-5-amino-3-methyl-1-(phenylsulfonyl)indole

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / pyridine / tetrahydrofuran / 8 h / Heating

2: 79 percent / lead tetraacetate / CHCl₃ / 12 h / 25 °C

3: 54 percent / BF₃*Et₂O / CH₂Cl₂ / 1) -78 deg C, 12 h, 2) -20 deg C, 12 h

4: 1) OsO₄, NaIO₄, 2) H₂SO₄ (10percent in CH₂Cl₂) / 1) acetone, water, 25 deg C, 2) CH₂Cl₂, 25 deg C

With pyridine; lead(IV) acetate; sodium periodate; osmium(VIII) oxide; sulfuric acid; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1021/jo00291a059

Reference yield:

: 327060-18-4
N⁴-Benzoyl-N¹-(phenylsulfonyl)-1,4-diaminobenzene

: 124400-53-9
N⁵-Benzoyl-5-amino-3-methyl-1-(phenylsulfonyl)indole

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / lead tetraacetate / CHCl₃ / 12 h / 25 °C

2: 54 percent / BF₃*Et₂O / CH₂Cl₂ / 1) -78 deg C, 12 h, 2) -20 deg C, 12 h

3: 1) OsO₄, NaIO₄, 2) H₂SO₄ (10percent in CH₂Cl₂) / 1) acetone, water, 25 deg C, 2) CH₂Cl₂, 25 deg C

With lead(IV) acetate; sodium periodate; osmium(VIII) oxide; sulfuric acid; boron trifluoride diethyl etherate; In dichloromethane; chloroform;
DOI:10.1021/jo00291a059