C₄₁H₅₂N₁₀O₁₁S

Base Information

Chemical Name:C₄₁H₅₂N₁₀O₁₁S
CAS No.:334953-05-8
Molecular Formula:C₄₁H₅₂N₁₀O₁₁S
Molecular Weight:892.99
Hs Code.:

C<sub>41</sub>H<sub>52</sub>N<sub>10</sub>O<sub>11</sub>S

Synonyms:

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Chemical Property of C₄₁H₅₂N₁₀O₁₁S

Chemical Property:

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Technology Process of C₄₁H₅₂N₁₀O₁₁S

There total 9 articles about C₄₁H₅₂N₁₀O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872-85-5
pyridine-4-carbaldehyde

: 334953-05-8
C₄₁H₅₂N₁₀O₁₁S

Guidance literature:: Multi-step reaction with 10 steps

1: 81 percent / ZnCl₂ / diethyl ether; tetrahydrofuran / -30 - 0 °C

2: aq. HCl / ethanol

3: HCl

4: 23 percent / Et₃N; DMAP / dioxane

5: H₂; PtO₂ / ethanol; acetic acid; H₂O

6: tetrahydrofuran

7: 100 percent / HCl / ethanol

8: NMM / acetonitrile

9: 1N LiOH / ethanol

10: EDC; HOBt; NMM / acetonitrile

With 4-methyl-morpholine; hydrogenchloride; dmap; platinum(IV) oxide; lithium hydroxide; hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; zinc(II) chloride; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; water; acetic acid; acetonitrile; 1: Ugi reaction / 2: Hydrolysis / 3: Esterification / 4: Acylation / 5: Catalytic hydrogenation / 6: guanylation / 7: deprotection / 8: Acylation / 9: Hydrolysis / 10: coupling;
DOI:10.1016/S0960-894X(00)00105-0

Reference yield:

: ((R)-2-Amino-2-pyridin-4-yl-acetylamino)-acetic acid

: 334953-05-8
C₄₁H₅₂N₁₀O₁₁S

Guidance literature:: Multi-step reaction with 8 steps

1: HCl

2: 23 percent / Et₃N; DMAP / dioxane

3: H₂; PtO₂ / ethanol; acetic acid; H₂O

4: tetrahydrofuran

5: 100 percent / HCl / ethanol

6: NMM / acetonitrile

7: 1N LiOH / ethanol

8: EDC; HOBt; NMM / acetonitrile

With 4-methyl-morpholine; hydrogenchloride; dmap; platinum(IV) oxide; lithium hydroxide; hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; water; acetic acid; acetonitrile; 1: Esterification / 2: Acylation / 3: Catalytic hydrogenation / 4: guanylation / 5: deprotection / 6: Acylation / 7: Hydrolysis / 8: coupling;
DOI:10.1016/S0960-894X(00)00105-0

Reference yield:

: 735256-22-1
((R)-2-Amino-2-pyridin-4-yl-acetylamino)-acetic acid ethyl ester

: 334953-05-8
C₄₁H₅₂N₁₀O₁₁S

Guidance literature:: Multi-step reaction with 7 steps

1: 23 percent / Et₃N; DMAP / dioxane

2: H₂; PtO₂ / ethanol; acetic acid; H₂O

3: tetrahydrofuran

4: 100 percent / HCl / ethanol

5: NMM / acetonitrile

6: 1N LiOH / ethanol

7: EDC; HOBt; NMM / acetonitrile

With 4-methyl-morpholine; hydrogenchloride; dmap; platinum(IV) oxide; lithium hydroxide; hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; water; acetic acid; acetonitrile; 1: Acylation / 2: Catalytic hydrogenation / 3: guanylation / 4: deprotection / 5: Acylation / 6: Hydrolysis / 7: coupling;
DOI:10.1016/S0960-894X(00)00105-0