C₁₄H₂₀N₄O₂

Base Information

• Chemical Name: C₁₄H₂₀N₄O₂
• CAS No.: 1308292-44-5
• Molecular Formula: C₁₄H₂₀N₄O₂
• Molecular Weight: 276.338
• Mol file: 1308292-44-5.mol

Synonyms:

Chemical Property of C₁₄H₂₀N₄O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₀N₄O₂

There total 2 articles about C₁₄H₂₀N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzaldehyde (100-52-7) → C14H20N4O2 (1308292-44-5)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 20 °C / Inert atmosphere

2: ethanol / 20 °C / Cooling with ice

With hydrazine hydrate; In ethanol;

DOI:10.1080/00397911.2010.525678

Reference yield:

2-(N-t-butoxycarbonylamino)thioacetamide (89226-13-1) → C14H20N4O2 (1308292-44-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone / 20 °C / Cooling with ice

2: ethanol / 20 °C / Cooling with ice

In ethanol; acetone;

DOI:10.1080/00397911.2010.525678

Reference yield: 50.0%

C14H20N4O2 (1308292-44-5) + C17H22N2O2 → C29H32N4O4 (1308292-57-0)

Guidance literature:

In toluene; for 3h; regioselective reaction; Reflux;

DOI:10.1080/00397911.2010.525678

upstream raw materials:

benzaldehyde

2-(N-t-butoxycarbonylamino)thioacetamide

Downstream raw materials:

C₂₉H₃₂N₄O₄