Technology Process of C23H34O5
There total 12 articles about C23H34O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
osmium(VIII) oxide; 4-methylmorpholine N-oxide;
In
water; acetone; tert-butyl alcohol;
for 22h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 29 percent / BF3*Et2O / CH2Cl2 / 240 h / Ambient temperature
2: 79 percent / p-toluenesulfonic acid / benzene / 4 h / Heating
3: 1.) BH3, 2-methyl-2-butene, 2.) 3N NaOH, 30percent H2O2 / 1.) THF, 0 deg C, 2 h, 2.) THF, H2O, 0-10 deg C
4: 83 percent / 50percent NaH / n-Bu4N(1+)*I(1-) / hexamethylphosphoric acid triamide / 24 h / Ambient temperature
5: 92 percent / OsO4, N-methylmorpholine-N-oxide / acetone; H2O; 2-methyl-propan-2-ol / 22 h / Ambient temperature
With
sodium hydroxide; osmium(VIII) oxide; 2-methyl-but-2-ene; boron trifluoride diethyl etherate; borane; dihydrogen peroxide; sodium hydride; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide;
tetra-(n-butyl)ammonium iodide;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; acetone; tert-butyl alcohol; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 83 percent / 50percent NaH / n-Bu4N(1+)*I(1-) / hexamethylphosphoric acid triamide / 24 h / Ambient temperature
2: 92 percent / OsO4, N-methylmorpholine-N-oxide / acetone; H2O; 2-methyl-propan-2-ol / 22 h / Ambient temperature
With
osmium(VIII) oxide; sodium hydride; 4-methylmorpholine N-oxide;
tetra-(n-butyl)ammonium iodide;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; water; acetone; tert-butyl alcohol;