Technology Process of 1-(Non-1-EN-1-YL)piperidine
There total 1 articles about 1-(Non-1-EN-1-YL)piperidine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(S,S)-5,11,17,23-tetra-tert-butyl-25,27-dipropyloxy-26,28-bis(1,1'-binaphthyl-2,2'-dioxyphosphanyloxy)calix[4]arene; C95H97O10P2Rh; hydrogen;
at 130 ℃;
for 1h;
under 15001.5 Torr;
Autoclave;
Neat (no solvent);
DOI:10.1039/c0gc00098a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Et3N / hexane / 2 h / under 50 deg C
2: 57percent aq. HClO4 / ethanol / 1.)r.t., 2 h 2.)0 deg C, 8 h
3: 74 percent / NH4OAc / acetic acid / 2 h / Heating
4: 85 percent / 220 - 240 °C
With
perchloric acid; ammonium acetate; triethylamine;
In
ethanol; hexane; acetic acid;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Et3N / hexane / 2 h / under 50 deg C
2: 57percent aq. HClO4 / ethanol / 1.)r.t., 2 h 2.)0 deg C, 8 h
3: 74 percent / NH4OAc / acetic acid / 2 h / Heating
With
perchloric acid; ammonium acetate; triethylamine;
In
ethanol; hexane; acetic acid;
