(η5-C5H5)(η5-C5H4(CH2)2P(cyclohexyl)2)TiCl2

Base Information

Chemical Name:(η5-C5H5)(η5-C5H4(CH2)2P(cyclohexyl)2)TiCl2
CAS No.:438206-39-4
Molecular Formula:C₂₄H₃₅Cl₂PTi
Molecular Weight:473.302
Hs Code.:

Synonyms:

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Chemical Property of (η5-C5H5)(η5-C5H4(CH2)2P(cyclohexyl)2)TiCl2

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Technology Process of (η5-C5H5)(η5-C5H4(CH2)2P(cyclohexyl)2)TiCl2

There total 1 articles about (η5-C5H5)(η5-C5H4(CH2)2P(cyclohexyl)2)TiCl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1270-98-0
cyclopentadienyl titanium(IV) trichloride

: 202843-37-6
lithium [(dicyclohexylphosphino)ethyl]cyclopentadienide

: 438206-39-4
(η5-C5H5)(η5-C5H4(CH2)2P(cyclohexyl)2)TiCl2

Guidance literature:: In tetrahydrofuran; ligand in THF was added to Ti-complex in THF, stirred for 4 h at room temp. under Ar; solvent was removed in vacuo, extd. with CH2Cl2, filtered, hexane was added, placed in freezer (-20°C) overnight, filtered, dried under vac.; elem. anal.;
DOI:10.1016/S0022-328X(01)01248-7

Reference yield: 90.0%

: 128706-72-9,658044-18-9,52462-29-0
[Ru(p-cymene)Cl₂]2

: 438206-39-4
(η5-C5H5)(η5-C5H4(CH2)2P(cyclohexyl)2)TiCl2

: (p-cymene)[(η5-C5H5)(μ-η5:η1-C5H4(CH2)2P(cyclohexyl)2)TiCl2]RuCl2

Guidance literature:: In benzene; Ti- and Ru-complexes were placed in flask with benzene under Ar, stirredat room temp. for 4 h; solvent was removed by filtration, dried under vac.; elem. anal.;
DOI:10.1016/S0022-328X(01)01248-7

Reference yield: 62.0%

: 532-32-1
sodium benzoate

: 438206-39-4
(η5-C5H5)(η5-C5H4(CH2)2P(cyclohexyl)2)TiCl2

: 882883-87-6
[Ti(O2CC6H5)2(η5-C5H5)(η5-C5H4(CH2)2P(C6H11)2)]

Guidance literature:: In water; toluene; under Ar, Schlenk setup, ligand and Ti compd. (2:1) in H2O:toluene=1:9, stirred for 1.5 h; org. phase washed (H2O), dried (MgSO4), filtered, evapd., elem. anal.;
DOI:10.1002/ejic.200401028