(((CH₃)3C₆H₂NCH₂)2C(CH₃)C₅H₄N)Zr(CH₃)2

Base Information

Chemical Name:(((CH₃)3C₆H₂NCH₂)2C(CH₃)C₅H₄N)Zr(CH₃)2
CAS No.:293764-40-6
Molecular Formula:C₂₉H₃₉N₃Zr
Molecular Weight:520.873
Hs Code.:

(((CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>NCH<sub>2</sub>)2C(CH<sub>3</sub>)C<sub>5</sub>H<sub>4</sub>N)Zr(CH<sub>3</sub>)2

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Chemical Property of (((CH₃)3C₆H₂NCH₂)2C(CH₃)C₅H₄N)Zr(CH₃)2

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Technology Process of (((CH₃)3C₆H₂NCH₂)2C(CH₃)C₅H₄N)Zr(CH₃)2

There total 2 articles about (((CH₃)3C₆H₂NCH₂)2C(CH₃)C₅H₄N)Zr(CH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 293764-38-2
[C₅H₄NC(CH₃)(CH₂NC₆H₂(CH₃)3)2]ZrCl₂

: 75-16-1
methylmagnesium bromide

: 293764-40-6
[(C₅H₄N)C(CH₃)(CH₂N(C₆H₂(CH₃)3))2]Zr(CH₃)2

Guidance literature:: In diethyl ether; N2; cooling of suspn. of Zr complex in diethyl ether to -30°C, addn. of 2.1 equiv. of methylmagnesium bromide as 3.4 M soln. in diethyl ether, stirring at room temp. for 15 min until the suspn. becomes clear; addn. of dioxane, filtering through Celite, reduction of solvent, crystn. at -30°C over 1 d; elem. anal.;
DOI:10.1021/om0207055

Reference yield:

: 293764-38-2
[(C₅H₄N)C(CH₃)(CH₂N(C₆H₂(CH₃)3))2]ZrCl₂

: 75-16-1
methylmagnesium bromide

: 293764-40-6
[(C₅H₄N)C(CH₃)(CH₂N(C₆H₂(CH₃)3))2]Zr(CH₃)2

Guidance literature:: In not given;
DOI:10.1021/ja000772v

Reference yield: 100.0%

: 60-29-7,927820-24-4
diethyl ether

: 293764-40-6
[(C₅H₄N)C(CH₃)(CH₂N(C₆H₂(CH₃)3))2]Zr(CH₃)2

: 917-54-4
methyllithium

: 486413-21-2
[C₅H₄NC(CH₃)(CH₂NC₆H₂(CH₃)3)2]Zr(methyl)3[Li*diethyl ether]

Guidance literature:: In diethyl ether; N2; addn. of methyllithium as 4.4 M ether soln. to ether suspn. of Zr complex at -30° C, stirring at room temp. for 10 min; filtration through Celite, drying the filtrate in vac.; elem. anal.;
DOI:10.1021/om0207055